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High-temperature anti-carburization anticorrosion infrared radiation glaze materials and method for preparing same

An infrared radiation and anti-carburizing technology, which is applied in the field of high temperature, carburizing and corrosion-resistant infrared radiation glaze and its preparation, can solve the problems of lack of high radiation function, harmful metal elements, unfavorable radiation heat transfer, etc. Improve the effect of anti-carburization and strengthen radiation heat transfer

Inactive Publication Date: 2006-09-27
武钢集团有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although it has strong radiation ability, is easy to sinter and is not easy to fall off, it has disadvantages: the use temperature is below 850°C, and the high infrared radiation area is limited to the 8-25μm far-infrared band, which is not conducive to radiation heat transfer at high temperatures
[0003] The high-temperature enamel coating technology introduced by the Ministry of Aviation Industry of my country from the former Soviet Union has finalized three products such as W-2, T-1 and B-1000 after years of experimental research by the Aeronautical Materials Research Institute. Its disadvantage: the substrate can only be nickel Cobalt alloy, the process is strict, and must be prepared in special equipment; it cannot be applied to civilian products
[0004] The high-temperature glazes released by the United States, Japan, South Korea and other countries, such as NBSA-19, etc., although the use temperature reaches 1000 ° C, are expensive, do not have high radiation function, and contain metal elements harmful to human body beryllium

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Apply the following glaze slurry to a metal substrate made of Cr25Ni35.

[0035] The glaze is composed of the following components and weight percentages: 9% flake glass frit, 17% ordinary glass frit, 16% enamel powder, 25% chromium oxide, 6% primer powder, 12% cordierite, high emissivity material 15%.

[0036] A method for preparing a high-temperature anti-carburization and anti-corrosion infrared radiation glaze, which sequentially includes the following steps:

[0037] 1), the above-mentioned flake glass frit 9%, ordinary glass frit 17%, enamel powder 16%, dichromium oxide 25%, down-leading powder 6%, cordierite 12%, high emissivity material 15% mix and grind Crushed, ball milled for 2 hours;

[0038] 2), filter out the grinding balls, let stand for 50 minutes, and remove the ball grinding fluid;

[0039] 3) Dry the ball mill wet material at a temperature of 135°C;

[0040] 4) Grind and sieve to make bone meal of 280-320 mesh, and store it for later use;

[0041...

Embodiment 2

[0044] Apply the following glaze slurry to a metal substrate made of Cr25Ni35.

[0045] The glaze is composed of the following components and weight percentages: 15% of flake glass frit, 15% of ordinary glass frit, 14% of enamel powder, 28% of chromium trioxide, 5% of primer powder, 10% of cordierite, high emissivity material 13%.

[0046] A method for preparing a high-temperature anti-carburization and anti-corrosion infrared radiation glaze, which sequentially includes the following steps:

[0047] 1), 15% of the above-mentioned flake glass frit, 15% of ordinary glass frit, 14% of enamel powder, 28% of dichromium trioxide, 5% of down-leading powder, 10% of cordierite, and 13% of high-emissivity material are mixed and ground Crushed, ball milled for 2.5 hours;

[0048] 2), filter out the grinding balls, let stand for 55 minutes, and remove the ball grinding liquid;

[0049] 3) Dry the ball mill wet material at a temperature of 150°C;

[0050] 4) Grind and sieve to make bo...

Embodiment 3

[0054] Apply the following glaze slurry to a metal substrate made of Cr25Ni35.

[0055] The glaze is composed of the following components and weight percentages: 23% of flake glass frit, 12% of ordinary glass frit, 12% of enamel powder, 26% of chromium trioxide, 5% of primer powder, 10% of cordierite, high emissivity material 12%.

[0056] A method for preparing a high-temperature anti-carburization and anti-corrosion infrared radiation glaze, which sequentially includes the following steps:

[0057] 1), 23% of the above-mentioned flake glass frit, 12% of ordinary glass frit, 12% of enamel powder, 26% of chromium trioxide, 5% of down-leading powder, 10% of cordierite, and 12% of high emissivity material are mixed and ground Crushed, ball milled for 2.5 hours;

[0058] 2), filter out the grinding balls, let stand for 58 minutes, and remove the ball grinding fluid;

[0059] 3) Dry the ball mill wet material at a temperature of 170°C;

[0060] 4) Grind and sieve to make bone ...

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PUM

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Abstract

The invention discloses a high temperature carbon-seepage-resistant corrosion prevention infrared radiation frit and preparing method, which comprises the following parts: 8-43% anticlinanthous plate, 10-17% simple frit, 10-17% enamel powder, 20-28% chrome green, 3-6% lower-guide-powder, 7-12% cordierite and 7-15% high emissivity material. The preparing method comprises the following steps: mixing up the above materials in the range of value and crushing; milling ball for two to three hours; filtering the mill-ball; stewing the mill-ball for 45 to 70 minutes and detaching the mill-ball liquid; drying the ball mill wet material at the temperature between 130deg.c and 200 deg.c; rolling for thin and riddling; preparing the 280-320 order bone mea. Preparing one kilo 600-800ml adhesive of high temperature infrared radiation frit and bone powder.

Description

technical field [0001] The invention relates to a high-temperature infrared radiation enamel glaze, especially a high-temperature anti-carburization and corrosion-resistant infrared radiation glaze with high emissivity in the full infrared band and its preparation, which is sintered on a heat-resistant metal heating body at 850-1200°C method. Background technique [0002] In recent years, various low and medium temperature infrared radiation glaze materials have been developed rapidly. For example, the Chinese Patent Publication No. CN1463940A "High Radiation Far Infrared Sintering Glaze" discloses a component and parts by weight of frit 40-90 , silicon carbide 0-10, calcined sand 2-12 and its oxide with infrared radiation performance 5-30, clay 3-15. Although it has strong radiation ability, is easy to sinter and is not easy to fall off, it has disadvantages: the use temperature is below 850°C, and the high infrared radiation area is limited to the 8-25μm far-infrared band...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C8/14C03C8/22
Inventor 朱小平蒋扬虎应宏刘萍陈健康欧阳德刚刘占增丁翠娇黄煊官赖为民马卫东张道明
Owner 武钢集团有限公司
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