Method for sufficient releasing effective component of ganoderma glossy ganoderma spore powder

A technology of Ganoderma lucidum spore powder and active ingredients, which can be used in medical preparations containing active ingredients, plant/algae/fungus/moss ingredients, and devices that make medicines into special physical or ingestible forms, and can solve the problem of damage to active ingredients , loss, difficult spore powder wall breaking treatment and other problems, to achieve high extraction rate, increase release rate, and improve extraction rate

Inactive Publication Date: 2006-04-12
SHENYANG KESI HIGH TECH +1
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] However, when the water content in the cell is too low, the raw material cannot be heated rapidly because it cannot fully absorb microwave energy, or the cell wall is strong enough, the "implosion" phenomenon is either difficult to occur, or it will not cause the cell wall to rupture; In this case, microwave extraction not only cannot play an efficient and fast role, but will cause the loss of active ingredients due to thermal damage
Since the water content in Ganoderma lucidum spore powder is generally not more than 10%, and the cell wall is extremely tough, it is difficult to use the "implosion" effect to break the spore powder, so it is also difficult to significantly increase the content of active ingredients in the spore powder by using microwave extraction technology. extraction efficiency

Method used

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  • Method for sufficient releasing effective component of ganoderma glossy ganoderma spore powder
  • Method for sufficient releasing effective component of ganoderma glossy ganoderma spore powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] ① 1.5kg Ganoderma lucidum spore powder is placed in a traveling wave microwave cavity;

[0027] ②Take 180g of oxalic acid and add 2.0L of water to make an oxalic acid solution;

[0028] ③Take 2L of the above solution, add it to the above microwave cavity, stir well to make it evenly wet;

[0029] ④The above materials are irradiated under 5KW continuous microwave power until there is liquid reflux, that is, the organic acid solution is vaporized, and the working mode is changed to pulsed microwave power. The duty cycle is 5 seconds / 5 seconds, the peak power is 10KW, and after 20 minutes, vacuumize (the working pressure of the reaction chamber is 20mmHg), until there is no liquid in the microwave chamber, the microwave softening treatment of the spore powder is completed.

[0030] ⑤ Add 5L of distilled water to 1.5kg of softened Ganoderma lucidum spore powder, stir well, filter, add calcium hydroxide solution to the filtrate until the oxalic acid precipitates completely,...

Embodiment 2

[0034] The difference from Example 1 is:

[0035] ① 1.5kg Ganoderma lucidum spore powder is placed in a traveling wave microwave cavity;

[0036] ② Take 1.8L of anhydrous formic acid and add 1.2L of water to make 3L of formic acid solution;

[0037] ③Take 3L of the above solution, add it to the above microwave cavity, stir well to make it evenly wet;

[0038] ④The above materials are irradiated under 3KW continuous microwave power until there is liquid reflux, that is, the organic acid solution is vaporized, and the working mode is changed to pulsed microwave power. The duty cycle is 5 seconds / 15 seconds, and the peak power is 8KW. After 40 minutes, vacuumize (The working pressure of the reaction chamber is 100mmHg) Distill under reduced pressure, get rid of the organic acid solution until there is no liquid in the microwave cavity, and complete the microwave softening treatment of the spore powder. Its polysaccharide release ability is shown in Table 1.

Embodiment 3

[0040] The difference from Example 1 is:

[0041] ①1.5kg Ganoderma lucidum spore powder is placed in a resonant microwave cavity;

[0042] ② Take 2.8L of anhydrous acetic acid and add 1.2L of water to make 4L of acetic acid solution;

[0043] ③Take 4L of the above solution, add it to the above microwave cavity, stir well to make it evenly wet;

[0044] ③The above materials are irradiated under 1KW continuous microwave power until there is liquid reflux, that is, the organic acid solution is vaporized, and the working mode is changed to pulsed microwave power. The duty cycle is 15 / 5 seconds, the peak power is 5KW, and after 60 minutes, vacuum ( The working pressure of the reaction chamber is 200 mmHg) under reduced pressure distillation, and the organic acid solution is removed until there is no liquid in the microwave chamber, and the microwave softening treatment of the spore powder is completed. Its polysaccharide release ability is shown in Table 1.

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Abstract

The invention relates to a processing technology of licuid ganoderma spore powder, in particular to a method for sufficient releasing licuid ganoderma spore powder. It adopts microwave softening treatment method. The concrete process is as follows: 1.placing raw materials licuid ganoderma spore powder into the microwave reaction chamber, adding organic acid solution and stirring sufficiently to make them wet homogenously 2.microwave treatment, applying microwave power to strengthen the reaction between the organic acid solution with chitin of the spore coat structure and colloid, enabling them partial solved and producing dense distributed nanometer holes or cracks on the spore coat. 3. vacuum distilling and removing organic acid solution. Said microwave power applying method combines he continuous microwave and impulse microwave, at first continuous microwave is applied to radiate, then the impulse microwave is applied when the organic acid solution refluxes, the irradiation time is 5min to 100min. The invention not only promotes the release capability of the effective constituent(in particular for polysaccharide) in the spore powder, but also ensures the integrity of the integral appearance of the spore powder. The loss of the easy oxidation effective constituent is also avoided.

Description

technical field [0001] The invention relates to the processing technology of ganoderma lucidum spore powder, in particular to a method capable of fully releasing the active ingredients of ganoderma lucidum spore powder. Background technique [0002] Ganoderma lucidum has been hailed as the "immortal herb" for strengthening the body and strengthening the foundation by Chinese medical scientists of all dynasties. In the past two decades, due to the success and vigorous promotion of artificial cultivation of Ganoderma lucidum, a lot of work has been done on the fruiting body and mycelium of Ganoderma lucidum. At the same time, the continuous improvement of the collection technology of Ganoderma lucidum spore powder has also greatly promoted people's systematic research on the pharmacological effects of the spore powder. Ganoderma lucidum spore powder is the species released by the ejection of Ganoderma lucidum in the later stage of development. Biologically, it is called basid...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/074A61J3/00
Inventor 张劲松李明天刘强
Owner SHENYANG KESI HIGH TECH
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