Water area up-conversion fluorescence vortex detection device and detection method thereof
A detection device and detection method technology, which are applied in measurement devices, fluorescence/phosphorescence, open-air water source survey, etc., can solve problems such as poor confidentiality, long delay, Doppler dispersion, etc., to improve accuracy and sensitivity, and reduce luminescence. Loss, Enhanced Detectability Effect
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Embodiment 1
[0042] Such as figure 1 As shown, the present invention provides a water area up-conversion fluorescence vortex detection device, which is a water area up-conversion fluorescence vortex detection device based on the principle of up-conversion luminescence and optics, installed on an aircraft, including a casing, a laser emitter , a nanoparticle storage bin and an image acquisition and processing system. The image acquisition and processing system includes an image acquisition module, an image processing module and an image display module.
[0043] The laser transmitter is connected to the image acquisition module, and emits infrared laser light in the direction to be detected for irradiation.
[0044] The nanoparticle storage bin is connected to the image acquisition module, and launches projectiles equipped with hydrophilic upconversion nanopowders in the direction to be detected. The projectiles blast in the designated area to release upconversion nanoparticles.
[0045] A...
Embodiment 2
[0051] Such as figure 2 Shown, on the basis of embodiment 1, the present invention provides a kind of detection method of water area up-conversion fluorescent vortex detection device, comprises the following steps carried out in order:
[0052] 1) The laser transmitter mounted on the aircraft emits infrared laser light in the direction to be detected for irradiation.
[0053] 2) The built-in magazine (nanoparticle storage bin) of the aircraft fires projectiles filled with hydrophilic upconversion nanopowders in the direction to be detected, and the projectiles blast in the designated area to release upconversion nanoparticles.
[0054] 3) The up-conversion nanoparticles emit visible light under the excitation of the infrared laser beam, presenting an optical image.
[0055] 4) The image acquisition and processing system carried by the aircraft collects optical images, which are processed to determine the turbulent conditions of the waters.
[0056] In this embodiment, the l...
Embodiment 3
[0064] On the basis of Example 2, the present invention also provides a hydrophilic Nd 3+ The preparation method of sensitized nanoparticles adopts high-temperature co-precipitation method to prepare monodisperse lanthanide ion-doped NaYF 4 Upconverting nuclear nanoparticles. Subsequently, NaYF was coated on the surface of core nanoparticles by epitaxial layer growth method. 4 inert shell. Concrete preparation steps are as follows:
[0065] 1) Synthesis of NaYF 4 :Nd 3+ ,Yb 3+ ,Er 3+ nuclear nanoparticles
[0066] (1) At room temperature (23-25°C), use a pipette to draw 3ml of OA (oleic acid), 7ml of ODE (1-octadecene), 2ml of Ln (CH 3 CO 2 ) 3 (0.2M) aqueous solution into a 50ml two-necked flask (add high-temperature magnets);
[0067] (2) Place the two-necked flask in an oil bath, set the temperature of the heating device to 130°C, and after the water in the liquid in the two-necked flask is completely evaporated, raise the temperature to 150°C and keep the temper...
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