Anti-fingerprint film, glass product and preparation method thereof

An anti-fingerprint film and glass product technology, which is applied in vacuum evaporation coating, coating, sputtering coating, etc., can solve the problem of weakened bonding strength between the film layer and the glass substrate, low friction resistance of the anti-fingerprint film, film Layer detachment from the base material and other problems, to achieve the effect of eliminating the problem of charge accumulation, long bonding strength, and simple process

Active Publication Date: 2021-07-20
LENS TECH CHANGSHA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the field of touch panels, the anti-fingerprint film applied on the glass substrate (especially the strengthened glass substrate) has low friction resistance, resulting in a short service life, which needs to be improved and improved
The main problem is that the glass substrate, especially the strengthened glass substrate, basically does not have conductivity. In actual use, due to external factors such as film coating / tearing, frequent operation and friction, a large amount of charge accumulates on the surface of the anti-fingerprint film layer. In turn, the bonding strength between the film layer and the glass substrate is weakened, and the film layer is separated from the substrate during frictional use, which accelerates the failure of the film layer

Method used

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  • Anti-fingerprint film, glass product and preparation method thereof
  • Anti-fingerprint film, glass product and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0063] A method for preparing the glass product, comprising:

[0064] The conductive film layer, the transition layer, the silicon dioxide layer and the anti-fingerprint film layer are sequentially prepared on the glass substrate by magnetron sputtering.

[0065] In an optional embodiment, the initial vacuum of the magnetron sputtering is less than or equal to 5.0e -3 Pa;

[0066] In an optional embodiment, an ion source treatment is performed on the surface of the glass substrate before preparing the conductive film layer;

[0067] In an optional embodiment, the ion source operating voltage of the primary ion source treatment is 800-1200V, the current is 0.8-2.0A, and the treatment time is 5-15min;

[0068] Optionally, the ion source operating voltage for the primary ion source treatment can be any value between 800V, 900V, 1000V, 1100V, 1200V, and 800-1200V; the ion source operating current for the primary ion source treatment can be 0.8A , 1.0A, 1.5A, 2.0A and any value ...

Embodiment 1

[0088] In this embodiment, the glass product of the front cover of the mobile phone made of AGC material is selected, and the initial water drop angle of the glass product before coating is measured after the two cleaning processes described in the present invention (see Table 1).

[0089] Place the cleaned glass products in a vacuum coating machine for coating. The specific process conditions are as follows:

[0090] 1. Vacuuming, the initial vacuum is 5.0e -3 Pa;

[0091] 2. Primary ion source treatment: using a linear ion source, under the condition of argon gas flow rate of 300 sccm and oxygen flow rate of 70 sccm, the plasma bombardment glass surface is generated at a voltage of 1000 V to clean the glass surface, and the processing time is 600 s , the actual output current is about 1.0 A;

[0092] 3. Conductive film layer: tin-indium alloy metal target, target power 4500 W, argon gas flow rate 300 sccm, oxygen flow rate 20 sccm, coating time 120s;

[0093] 4. Transiti...

Embodiment 2

[0101] The sample of this example was prepared by the same method as in Example 1, wherein the coating time of the conductive film layer was 65 s, the coating time of silicon dioxide was 500 s, and the rest of the conditions were unchanged.

[0102] In this embodiment, the thickness of the single layer is measured by a scanning electron microscope, wherein the thickness of the conductive film layer is about 3nm, the thickness of the transition layer is about 3nm, and the thickness of the SiO 2 The thickness of the layer is about 8nm, and the thickness of the anti-fingerprint film is about 24.6 nm. See Table 1 for the water drop angle of glass products after coating.

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Abstract

The invention provides an anti-fingerprint film, a glass product and a preparation method thereof. The anti-fingerprint film includes a conductive film layer, a transition layer, a silicon dioxide layer, and an anti-fingerprint film layer that are stacked in sequence; the conductive film layer includes one of In, In oxides, Sn, Sn oxides, or Various, the transition layer includes Si 3 N 4 , SiON and SiO 2 . The glass product includes a glass substrate and the anti-fingerprint film; the substrate is adjacent to the conductive film layer. The method for preparing glass products includes: sequentially preparing the conductive film layer, the transition layer, the silicon dioxide layer and the anti-fingerprint film layer on a glass substrate by magnetron sputtering. The anti-fingerprint film provided by the present application has excellent friction resistance, waterproof and anti-fingerprint properties, and has a long service life.

Description

technical field [0001] The invention relates to the field of glass products, in particular to an anti-fingerprint film, glass products and a preparation method thereof. Background technique [0002] In order to improve customer experience, a layer of anti-fingerprint film is usually applied to the panel glass of mobile phones and tablets to improve the anti-fouling and lubricating properties of the glass panel. This technology has attracted people's attention. In the field of touch panels, the anti-fingerprint film applied on the glass substrate (especially the strengthened glass substrate) has low friction resistance, resulting in a short service life, which needs to be improved and improved. The main problem is that the glass substrate, especially the strengthened glass substrate, basically does not have conductivity. In actual use, due to external factors such as film coating / tearing, frequent operation and friction, a large amount of charge accumulates on the surface of ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/18C23C14/35C23C14/02C23C14/10C23C14/24C23C14/06C23C14/54
CPCC23C14/0036C23C14/022C23C14/06C23C14/0652C23C14/0676C23C14/10C23C14/185C23C14/24C23C14/35C23C14/54
Inventor 周群飞刘谋苗
Owner LENS TECH CHANGSHA
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