Production method of high-purity aluminum oxide and produced high-purity aluminum oxide
A high-purity alumina, production method technology, applied in alumina/hydroxide preparation, hydrogen production, chemical instruments and methods, etc., can solve the problems of high cost, serious equipment corrosion, difficult industrialization, etc.
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Embodiment 1
[0034] Weigh 400g of 4N metal aluminum ingot with an aluminum content of 99.99wt%, and also weigh 0.04g of gallium and indium (including 0.0316g of gallium and 0.0084g of indium), and place them in a stirred medium frequency vacuum melting furnace. 1.0~1.0×10 -1 Under the condition of Pa, smelt at 800℃ for 30min, stir continuously during the smelting, the stirring speed is 300 rpm, and then cast into the mold, after natural cooling, the aluminum ingot is obtained, and the aluminum ingot is cut and refined into particles below 1 cm. The mass ratio of aluminum gallium indium is: 100:0.0079:0.0021, gallium indium accounts for 0.01wt% of the total metal mass; add 8L of pure water into the pressurized reactor, heat it to 95°C, add aluminum particles while stirring, continue heating to make water Boiling; as the reaction between aluminum and water progresses, the gas pressure in the reactor rises, the gas is led out of the supercooled hydrazine, the water is separated, and the hydroge...
Embodiment 2
[0036] Weigh 400g of 5N metal aluminum ingot with an aluminum content of 99.999wt%, and also weigh 0.8g of metal gallium and indium (including 0.632g of gallium and 0.168g of indium), and place them in a stirred argon-protected melting furnace. ×10 5 Under the condition of Pa, smelt at 800°C for 30 minutes, stirring at a stirring speed of 300 revolutions / min, and then pouring into a mold. The aluminum ingot is cut and refined into particles below 1 cm. The mass ratio of aluminum gallium indium in the aluminum ingot is: 100:0.158:0.042, gallium and indium accounted for 0.2wt% of the total metal mass; add 8L of pure water into the pressurized reactor, heat it to 95℃, add aluminum particles while stirring, and continue heating to make the water boil; as the aluminum and water As the reaction progresses, the gas pressure in the reactor rises, the gas is led out of the supercooled hydrazine, the water is separated and removed, and the hydrogen is collected; after the aluminum-water r...
Embodiment 3
[0038] Weigh 400g of 5N metal aluminum ingot with an aluminum content of 99.999wt%, and also weigh 0.40g of gallium and indium (including 0.316g of gallium and 0.084g of indium), and place them in a stirred intermediate frequency vacuum melting furnace. Under the condition of 1.0~1.0×10-1Pa, smelt at 800℃ for 30min, and stir continuously during the stirring at 300 rpm. Then, it is poured into a mold, and the aluminum ingot is cut and refined into particles below 1 cm. The aluminum ingot contains aluminum The mass ratio of gallium to indium is: 100:0.079:0.021, and gallium indium accounts for 0.1wt% of the total metal mass; add 8L of pure water into the pressurized reactor, heat to 95℃, add aluminum particles while stirring, continue heating to make the water boil ; As the reaction between aluminum and water progresses, the gas pressure in the reactor increases, the gas is led out of the supercooled hydrazine, the water is separated, and the hydrogen is collected; the aluminum-wa...
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