Spray-coating damping coating for ships and preparation method= thereof
A technology for damping coatings and ships, applied in anti-corrosion coatings, fire-proof coatings, epoxy resin coatings, etc., can solve the problems of not meeting the requirements of lightweight, low composite loss factor, high density of damping materials, etc., and achieve high composite loss factor , Excellent flame retardant performance, excellent sound insulation effect
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[0084] In addition, the present invention also provides a method for preparing the above-mentioned sprayable damping coating for ships, including:
[0085] Preparation of the A component: heat the diisocyanate to 50-60°C, add the polyol dropwise to it, and keep the above temperature range while stirring; after the dropwise addition, raise the temperature to 80-95°C , heat preservation reaction for 2 to 4 hours, and after the NCO content reaches the target value of 3.0 to 7.0 wt%, the temperature is lowered to 40 to 50°C to obtain the first component;
[0086] Preparation of the B component: sequentially add the chain extender and the polyol into the reaction kettle and raise the temperature to 50-60°C, then add the damping modifier and then raise the temperature to 80°C, keep warm for 1- After 2 hours of filling and dissolving the damping modifier, lower the temperature to below 50°C and transfer it to a high-speed disperser; then add the dispersant, defoamer, substrate wettin...
Embodiment 1
[0096] 1. Preparation of damping layer
[0097] 1.1 Preparation process of damping layer A component
[0098] Heat 65 parts of TDI to 50-60°C, add 250 parts of polyether DL1000 dropwise to it, and keep the above temperature range while stirring; after the addition is completed, raise the temperature to 80-90°C, keep the temperature for 2-3 hours, and lower the temperature A prepolymer with an NCO content of 3.28% can be obtained when the temperature is lowered to 40-50°C.
[0099] 1.2 Preparation process of component B of the damping layer
[0100] (1) Add 40 parts of chain extender 1,4-butanediol and 150 parts of DL400 to the reaction kettle in turn and raise the temperature to 50-60°C, then add 50 parts of damping modifier AO-80 and the temperature rises to 80°C , keep warm for 1-2h, after the damping modifier is fully dissolved, lower the temperature to below 50°C for later use;
[0101] (2) The material prepared in step (1), 10 parts of dispersant BYK110, 1 part of defo...
Embodiment 2
[0113] 1. Preparation of damping layer
[0114] 1.1 Preparation process of damping layer A component
[0115] Heat 150 parts of MDI-50 to 50-60°C, add 200 parts of polycaprolactone Placcel205U dropwise to it, and maintain the above temperature range while stirring; after the addition is completed, raise the temperature to 80-90°C, and keep warm for 2~ After 3 hours, the temperature was lowered to 40-50°C to obtain a prepolymer with an NCO content of 5.34%.
[0116] 1.2 Preparation process of component B of the damping layer
[0117] (1) Add 40 parts of chain extender E300 and 100 parts of PCL1000 to the reaction kettle in sequence and raise the temperature to 50-60°C, then add 78 parts of damping modifier AO-80 and then the temperature rises to 80°C, keep it warm for 1-2 hours After the damping modifier is fully dissolved, lower the temperature below 50°C for later use;
[0118] (2) The material prepared in step (1), 5 parts of dispersant Tego610, 2 parts of defoamer Foamex...
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