A kind of two-dimensional plzst antiferroelectric photonic crystal and its preparation method
A photonic crystal and antiferroelectric technology, applied in optics, nonlinear optics, instruments, etc., can solve the problems of many defects in photonic crystals, low electron mobility and breakdown field strength, no obvious changes, etc., and achieve accurate optical parameters , Precise parameters, regular shape effect
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[0039] like figure 1 As shown in the two-dimensional photoelectron PLZST antiferromagnetic preparation method provided in the crystals embodiment of the present invention comprises:
[0040] (1) selecting n-propoxide, zirconium, tetrabutyl titanate, lead acetate, tin acetate, lanthanum nitrate as raw materials, acetic acid, ethylene glycol ethyl ether, acetyl acetone, formamide as solvent preparation methods PLZST Sol-Gel sol.
[0041] (2) the SSO template immobilized on a spin coater, PLZST sol dropwise, filled SSO template using a spin coating method.
[0042] (3) first in an electrically heated hot plate, the heating temperature is set at 60-80 deg.] C, at continued at 80 ℃ 15min.
[0043] (4) After cooling the sample is fixed on a spin coater, a spin-coating a second fill, repeat step (3).
[0044] (5) Repeat step (4) 4 to 5 times.
[0045] (6) The sample was placed in a tube furnace and purged with argon, sintered, and then naturally cooled.
[0046] (7) The sample was taken,...
Embodiment
[0060] like image 3 As shown, a method of preparing a two-dimensional PLZST anti-ferrous photoelectric sub-crystal according to an embodiment of the present invention.
[0061] Figure 4 A method of preparation of an SSO template according to an embodiment of the present invention.
[0062] Figure 5 It is a top view of a two-dimensional PLZST anterior iron electro-photocylet crystal attached to a silicon substrate provided by the embodiment of the present invention.
[0063] The SEM diagram of the experimental sample of the present invention has a photonic crystal pore diameter of 500 nm. When the measurement error is ignored, the pore diameter of the photonic crystal air column is almost the same, and the deviation from the experimental design parameters can be ignored. From the perspective of realization, the two-dimensional PLZST photonic crystal prepared by the method provided by the present invention has the precision of parameters, the shape rules, and the structure is comp...
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