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A kind of preparation method of thin sheet type rare earth permanent magnet material

A rare earth permanent magnet and chip technology, which is applied in the direction of magnetic materials, inductance/transformer/magnet manufacturing, magnetic objects, etc., can solve the problems of shortened service life, easy corrosion at grain boundaries, poor wear resistance, etc.

Active Publication Date: 2021-05-07
安吉县宏铭磁性器材有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, although metal alloy magnets and ferrite magnetic materials have the advantages of low cost and abundant raw materials, their maximum magnetic energy product (BH)max is generally less than 10MGOe, and their magnetic properties are poor, so they are gradually replaced by rare earth permanent magnet materials.
[0007] The permanent magnet materials in the prior art have low bending strength, poor wear resistance, and limited corrosion resistance. When used for a long time, the grain boundaries will be easily corroded, and the magnetism will be destroyed during long-term use, shortening the service life.

Method used

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  • A kind of preparation method of thin sheet type rare earth permanent magnet material

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Embodiment 1

[0026] A preparation method of a thin sheet type rare earth permanent magnet material, comprising the following steps:

[0027] (1) Preparation of the main phase alloy. After mixing 11 parts of elemental neodymium, 0.4 parts of elemental dysprosium, 65 parts of elemental iron, and 4 parts of elemental boron, the main phase alloy was prepared, and then crushed, ground, and sieved to obtain the main phase alloy. gold powder;

[0028] (2) Preparation of grain boundary phase alloys, mixing 26 parts of elemental neodymium, 0.5 parts of Co, 0.5 parts of Mo, 4.3 parts of boron, and 45 parts of iron for rapid solidification, with a quenching rate of 27m / s, to prepare a grain boundary alloy , and then pulverized to obtain grain boundary phase alloy powder;

[0029] (3) Mix the main phase alloy powder, grain boundary phase alloy powder, magnesium oxide and zinc oxide evenly according to the mass ratio of 10:0.6:0.3:0.4, then mold them into a sheet-like green embryo, and put the green e...

Embodiment 2

[0031] A preparation method of a thin sheet type rare earth permanent magnet material, comprising the following steps:

[0032] (1) Preparation of the main phase alloy. After mixing 13 parts of elemental neodymium, 0.7 parts of elemental dysprosium, 73 parts of iron oxide, and 6 parts of elemental boron, the main phase alloy was prepared, and then crushed, ground, and sieved to obtain the main phase alloy. gold powder;

[0033] (2) Preparation of the grain boundary phase alloy, mixing 28 parts of elemental neodymium, 1 part of Co, 1 part of Mo, 5.5 parts of boron, and 52 parts of iron oxide, and then rapid solidification, the quenching rate is 35m / s, and the grain boundary is prepared alloy, then pulverized to obtain grain boundary phase alloy powder;

[0034] (3) Mix the main phase alloy powder, grain boundary phase alloy powder, magnesium oxide, and zinc oxide according to the mass ratio of 10: 1.5: 0.8: 0.8, then mold them into a sheet-shaped green embryo, and put the gree...

Embodiment 3

[0036] A preparation method of a thin sheet type rare earth permanent magnet material, comprising the following steps:

[0037] (1) Preparation of the main phase alloy. After mixing 12 parts of elemental neodymium, 0.5 part of elemental dysprosium, 70 parts of iron oxide, and 5 parts of elemental boron, the main phase alloy is prepared, and then crushed, ground, and sieved to obtain the main phase alloy. Gold powder, included in the main phase alloy by parts by weight. ;

[0038] (2) Preparation of grain boundary phase alloys, mixing 27 parts of neodymium, 0.6 parts of Co, 0.7 parts of Mo, 5 parts of boron, and 47 parts of iron for rapid solidification, the quenching rate is 30m / s, and prepared into grain boundary alloys. Pulverize then, obtain grain boundary phase alloy powder;

[0039] (3) Mix the main phase alloy powder, grain boundary phase alloy powder, magnesium oxide, and zinc oxide evenly according to the mass ratio of 10:1:0.5:0.5, then mold them into a sheet-shaped...

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Abstract

The invention improves a preparation method of a thin sheet type rare earth permanent magnet material, and relates to the technical field of magnetic materials. A method for preparing a thin sheet-type rare earth permanent magnet material, comprising the following steps: (1) Preparation of a main phase alloy, mixing materials containing neodymium, dysprosium, iron, and boron respectively to prepare a main phase alloy, and then pulverizing , grinding, and sieving to obtain the main phase alloy powder; (2) preparation of the grain boundary phase alloy, mixing materials containing neodymium, Co, Mo, boron, and iron respectively, and then performing rapid solidification, and the quenching rate is 27-35m / s, prepare a grain boundary alloy, and then pulverize it to obtain a grain boundary phase alloy powder; (3) Mix the main phase alloy powder, grain boundary phase alloy powder, magnesium oxide, and zinc oxide evenly, then perform molding, press into a sheet-shaped green embryo, and then Sintering, cooling after tempering to obtain thin sheet type rare earth permanent magnet material. According to the preparation method of the thin sheet type rare earth permanent magnet material of the present invention, the prepared rare earth permanent magnet material has excellent magnetic properties, high bending strength and strong corrosion resistance.

Description

technical field [0001] The invention relates to the technical field of magnetic materials, in particular to a preparation method of a thin sheet type rare earth permanent magnet material. Background technique [0002] Permanent magnet materials are also called "hard magnetic materials". A material that maintains a constant magnetic field once magnetized. It has wide hysteresis loop, high coercive force and high remanence. In practice, permanent magnet materials work in the second quadrant demagnetization part of the hysteresis loop after deep magnetic saturation and magnetization. Commonly used permanent magnet materials are divided into AlNiCo permanent magnet alloys, FeCrCo permanent magnet alloys, permanent ferrites, rare earth permanent magnet materials and composite permanent magnet materials. [0003] Permanent magnet materials include ferrite permanent magnets, rare earth permanent magnets (rare earth cobalt, neodymium iron boron, etc.), alnico, iron chromium cobal...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01F41/02H01F1/057
CPCH01F1/0576H01F41/0253H01F41/0266H01F41/0293
Inventor 杨维铭
Owner 安吉县宏铭磁性器材有限公司
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