Method for filtering aquaculture sewage
A filtration method and aquaculture technology, which are applied in the fields of light water/sewage treatment, oxidized water/sewage treatment, water/sludge/sewage treatment, etc. The ability to release silver ions for a long time, the effect of broad-spectrum antibacterial effect
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Embodiment 1
[0062] Preparation of microporous membranes according to the invention:
[0063] materials needed:
[0064] (1) Porous substrate: a pre-washed clean microporous polyethersulfone substrate; the porosity of the substrate is 50.1%, and the average pore diameter is 0.1 micron;
[0065] (2) Sensitization solution: 10 grams of SnCl 2 2H 2 O was mixed with 40 mL of 37% hydrochloric acid and the final volume of the mixture was brought to 1 L with deionized water;
[0066] (3) Activation solution: Mix 10 grams of silver nitrate with 10 mL of ammonium hydroxide and make up to 1 liter of final volume with deionized water;
[0067] (4) TiO 2 Powder: Nitrogen-doped TiO 2 Powder, the doping amount of nitrogen is 2.08at%.
[0068] Preparation:
[0069] (i) Immerse the pre-cleaned microporous polyethersulfone substrate in the sensitizing solution maintained at 25°C and 1 atmosphere for 20 minutes; remove the substrate from the sensitizing solution and rinse it in deionized water for 5 ...
Embodiment 2
[0073] Preparation of microporous membranes according to the invention:
[0074] materials needed:
[0075] (1) Porous matrix: a pre-washed clean microporous polysulfone matrix (Para MF membrane); the porosity of the matrix is 56.2%, and the average pore size is 0.26 microns;
[0076] (2) Sensitization solution: 10 grams of SnCl 2 2H 2 O was mixed with 40 mL of 38% hydrochloric acid and the final volume of the mixture was brought to 1 L with deionized water;
[0077] (3) Activation solution: Mix 10 grams of silver nitrate with 10 mL of ammonium hydroxide and make up to 1 liter of final volume with deionized water;
[0078] (4) TiO 2 Powder: co-doped TiO with phosphorus, nitrogen and molybdenum 2 Powder, the doping amount of phosphorus is 1.6 at%, the doping amount of nitrogen is 6.8 at%, and the doping amount of molybdenum is 3.2 at%.
[0079] Preparation:
[0080] (i) Immerse the pre-cleaned microporous polysulfone substrate in a sensitizing solution maintained at 25...
Embodiment 3
[0092]Utilize the microporous membrane to filter aquaculture sewage, the water purification effect is shown in Table 1; as can be seen from Table 1, the microporous membrane of the present invention can be effectively used in the filtration of aquaculture sewage, and after filtration, organic matter, bacteria, viruses, etc. in the sewage can be removed relatively complete; the introduction of ultrasonic waves in the filtration process can strengthen the degradation of organic matter by titanium dioxide; and the use of a mixed solution of resveratrol and isoamyl acetate to pretreat the microporous membrane is beneficial to affect the relationship between organic matter in sewage, and also Shows enhanced organic removal.
[0093] Table 1 water purification effect
[0094]
[0095] The conventional technologies in the above embodiments are known to those skilled in the art, so they will not be described in detail here.
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