High-niobium austenite heat-resistant steel having high tissue stability under 700 DEG C and preparation method of high-niobium austenite heat-resistant steel
An austenitic heat-resistant steel and stability technology, applied in the field of high-temperature metal structural materials, can solve problems such as poor organizational stability, threats to the safety of crew and personnel, and inability to meet service performance requirements.
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Embodiment 1
[0043] 1) Alloy preparation.
[0044] The specific chemical composition (unit: mass percentage) of the above alloy at the time of preparation is Cr: 21.5%, Ni: 18%, Nb: 1.7%, C: 0.04%, N: 0.1%, Co: 0.9%, Si: 0.4% , Mn:
[0045] 0.03%, B: 0.002%, Zr: 0.002%, and the balance is Fe.
[0046] After considering the burning loss, the batching is completed, argon gas is introduced into the vacuum arc melting furnace as a protective gas, and a 150g button ingot with uniform alloy composition is obtained by electromagnetic stirring and turning. In order to eliminate macroscopic and microscopic segregation, a homogenization annealing treatment is carried out at 1100-1260°C for 20-35 hours, so that the alloy elements can be diffused as fully and uniformly as possible. After the homogenization annealing treatment, in order to make a large amount of Nb, C and N elements in the primary MX phase dissolve back into the matrix as much as possible, the alloy is subjected to solution treatment...
Embodiment 2-7
[0056] Table 2 shows the specific chemical composition of the alloys of Examples 2-7 of the present invention. Through the preparation and analysis of these alloys, it is found that the corresponding microstructure stability and mechanical properties are in line with the conditions and requirements applied to the steam pipeline of the 650 ℃ ultra-supercritical supercritical super / reheater.
[0057] Table 2 Chemical composition of Examples 2-7 of the present invention (unit is mass percent, balance is Fe)
[0058] alloy
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