Abrasion-resistant glass based on micro-nano array structure coating and preparation method thereof
A wear-resistant glass, array structure technology, applied in the coating and other directions, can solve the problems of poor adhesion between the coating and the glass substrate, poor wear resistance of the coating, etc., to avoid volume shrinkage, improve density, and mild conditions.
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Embodiment 1
[0026] (1) Place the glass sheet in acetone and absolute ethanol successively for washing, dry it and place it in a concentrated sulfuric acid solution for etching treatment for 10 minutes, then take it out and wash it with clean water, dry it, and wait for treatment; silicon nitride powder and Mixed water and ethanol ball milling to obtain fine silicon nitride powder; then use plasma spraying technology to prepare a silicon nitride coating with a thickness of 100nm on the glass surface;
[0027] (2) The glass flakes that have been sprayed with a silicon nitride coating are cleaned with acetone and dried; the obtained mass concentration is 13% in an aqueous solution of zinc nitrate hexahydrate, and then 8% of the quality of zinc nitrate hexahydrate is added. Sodium acetate, continue to stir until the solid dissolves to obtain a mixed solution; put the mixed solution in a reaction kettle, add the cleaned glass sheet coated with silicon nitride coating; then add zinc nitrate hexahy...
Embodiment 2
[0031] (1) Place the glass sheet in acetone and absolute ethanol successively for washing, and after drying, place it in concentrated sulfuric acid solution for etching treatment for 30 minutes, then take it out and wash it with clean water, dry it, and wait for treatment; silicon nitride powder and Water and ethanol mixed ball milling treatment to obtain fine silicon nitride powder; then use plasma spraying technology to prepare a silicon nitride coating with a thickness of 200nm on the glass surface;
[0032] (2) The glass flakes that are sprayed with silicon nitride coating are cleaned with acetone and dried; the obtained mass concentration is 22% in the aqueous solution of zinc nitrate hexahydrate, and then 11% of the quality of zinc nitrate hexahydrate is added. Sodium acetate, continue to stir until the solid dissolves to obtain a mixed solution; put the mixed solution in a reaction kettle, add the cleaned glass sheet coated with silicon nitride coating; then add zinc nit...
Embodiment 3
[0036] (1) Place the glass sheet in acetone and absolute ethanol successively for washing, and after drying, place it in concentrated sulfuric acid solution for etching treatment for 20 minutes, then take it out and wash it with clean water, dry it, and wait for treatment; silicon nitride powder and Mixed water and ethanol ball milling to obtain fine silicon nitride powder; then use plasma spraying technology to prepare a silicon nitride coating with a thickness of 100nm on the glass surface;
[0037] (2) The glass flakes that have been sprayed with a silicon nitride coating are cleaned with acetone and dried; the obtained mass concentration is 15% in an aqueous solution of zinc nitrate hexahydrate, and then 9% of the quality of zinc nitrate hexahydrate is added. Sodium acetate, continue to stir until the solid dissolves to obtain a mixed solution; put the mixed solution in a reaction kettle, add the cleaned glass sheet coated with silicon nitride coating; then add zinc nitrate...
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