Normal-temperature nickel-free hole sealing agent
A technology of nickel sealing and normal temperature, which is applied in the direction of electrolytic coating, surface reaction electrolytic coating, coating, etc. It can solve the problems of large polymer resin molecular volume, inability to diffuse sealing performance, human body and environmental toxicity, etc., and achieve the elimination of bad Impact, energy saving, waste water non-toxic and harmless effect
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preparation example Construction
[0032] Another aspect of the present invention also provides a preparation method of the normal temperature nickel-free sealing agent, comprising the following steps:
[0033] (1) Mix the lithium salt and the sealing accelerator, add deionized water and stir evenly to obtain a solution;
[0034] (2) Add component D to the above solution, and stir for 1-1.5h under the condition of 250-300r / min to obtain a mixed solution;
[0035] (3) Add the pH buffering agent to the above mixed solution, stir and react at 30-35° C. for 2.5-3 hours to obtain a nickel-free sealing agent at room temperature.
[0036] The third aspect of the present invention also provides a method for using the normal temperature nickel-free sealing agent, comprising the following steps:
[0037] (1) Immerse the anodized aluminum alloy substrate in nickel-free sealing agent, the usage ratio is 20-40g / L, and the sealing speed is 1-1.5μm / min;
[0038] (2) Wash the residual sealing agent on the surface of the alum...
Embodiment 1
[0052] Example 1 provides a nickel-free sealing agent at room temperature. Calculated by mass percentage, the nickel-free sealing agent at room temperature includes the following components: 30% of lithium salt, 10% of pH buffer agent, 0.6% of sealing accelerator, Deionized water balance.
[0053] The normal temperature nickel-free sealing agent also includes 3% component D.
[0054] Wherein, the lithium salt is a composition of lithium acetate and lithium sulfate, the corresponding weight ratio is 1:1.35; the pH buffer is ammonium acetate; the sealing accelerator is dioctyl sodium sulfosuccinate The composition of salt and trimethylglycine, the corresponding weight ratio is 1:1; the component D is the composition of polyethylene glycol 600 and acrylic resin, the corresponding weight ratio is 1.1:1.8; The acrylic resin was purchased from Mitsubishi, Japan, and the model was BR113.
[0055] On the other hand, this embodiment also provides a preparation method of the normal te...
Embodiment 2
[0063] Example 2 provides a nickel-free sealing agent at room temperature. Calculated by mass percentage, the nickel-free sealing agent at room temperature includes the following components: 20% of lithium salt, 6% of pH buffer agent, 0.2% of sealing accelerator, Deionized water balance.
[0064] The normal temperature nickel-free sealing agent also includes 2% component D.
[0065] Wherein, the lithium salt is a composition of lithium acetate and lithium sulfate, the corresponding weight ratio is 1:1.35; the pH buffer is ammonium acetate; the sealing accelerator is dioctyl sodium sulfosuccinate The composition of salt and trimethylglycine, the corresponding weight ratio is 1:1; the component D is the composition of polyethylene glycol 600 and acrylic resin, the corresponding weight ratio is 1.1:1.8; The acrylic resin was purchased from Mitsubishi, Japan, and the model was BR113.
[0066] On the other hand, this embodiment also provides the preparation method of the nickel-f...
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