A kind of nickel foam in situ loading sno 2 Preparation method and application of nanoparticle-doped graphitic carbon composite material
A composite material and nanoparticle technology, applied in the fields of nanomaterials, nanocatalysis, and metal organic framework materials, can solve the problems of unreported research and high cost
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Embodiment 1
[0023] Example 1 A nickel foam in situ loading SnO 2 Preparation method of nanoparticle-doped graphitic carbon composite material
[0024] 0.165 g terephthalic acid H 2 Dissolve BDC and 0.30 g ferric nitrate nonahydrate in 8 mL DMF, add 0.08 g tin powder after ultrasonication for 3 min, and continue ultrasonication for 3 min to obtain a mixed solution;
[0025] In this mixed solution, the activated nickel foam NiF with an area of 1 cm×1 cm was used as the working electrode, the platinum sheet was used as the counter electrode, and the calomel electrode was used as the reference electrode, and the Sn(IV) / Fe(III)-BDC / NiF composite material;
[0026] The Sn(IV) / Fe(III)-BDC / NiF composite was heated to 250 °C at a heating rate of 2 °C / min in an air atmosphere, kept for 2 h, and then cooled at a cooling rate of 2 °C / min to room temperature; SnO 2 @C / NiF composite material, that is, Ni foam supports SnO in situ 2 Nanoparticle-doped graphitic carbon composites;
[0027]The ac...
Embodiment 2
[0032] Example 2 A nickel foam in situ loading SnO 2 Preparation method of nanoparticle-doped graphitic carbon composite material
[0033] 0.166 g terephthalic acid H 2 Dissolve BDC and 0.40 g ferric nitrate nonahydrate in 10 mL DMF, add 0.10 g tin powder after ultrasonication for 4 min, and continue ultrasonication for 4 min to obtain a mixed solution;
[0034] In this mixed solution, the activated nickel foam NiF with an area of 1 cm×1 cm was used as the working electrode, the platinum sheet was used as the counter electrode, and the calomel electrode was used as the reference electrode, and the Sn(IV) / Fe(III)-BDC / NiF composite material;
[0035] The Sn(IV) / Fe(III)-BDC / NiF composite was heated to 300 °C at a heating rate of 2 °C / min in an air atmosphere, kept for 2 h, and then cooled at a cooling rate of 2 °C / min to room temperature; SnO 2 @C / NiF composite material, that is, Ni foam supports SnO in situ 2 Nanoparticle-doped graphitic carbon composites;
[0036] The ...
Embodiment 3
[0040] Example 3 A nickel foam in situ loading SnO 2 Preparation method of nanoparticle-doped graphitic carbon composite material
[0041] 0.167 g terephthalic acid H 2 Dissolve BDC and 0.50 g ferric nitrate nonahydrate in 12 mL DMF, add 0.12 g tin powder after ultrasonication for 5 min, and continue ultrasonication for 5 min to obtain a mixed solution;
[0042] In this mixed solution, the activated nickel foam NiF with an area of 1 cm×1 cm was used as the working electrode, the platinum sheet was used as the counter electrode, and the calomel electrode was used as the reference electrode, and the Sn(IV) / Fe(III)-BDC / NiF composite material;
[0043] The Sn(IV) / Fe(III)-BDC / NiF composite was heated to 350 °C at a heating rate of 2 °C / min in an air atmosphere, kept for 2 h, and then cooled at a cooling rate of 2 °C / min to room temperature; SnO 2 @C / NiF composite material, that is, Ni foam supports SnO in situ 2 Nanoparticle-doped graphitic carbon composites. The activated...
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