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Basalt fiber preparation method, mineral mixture and production technology

A technology of basalt fiber and mixture, which is applied in the field of materials, can solve the problems of narrow source of raw materials, fluctuations in composition, costing a lot of manpower and financial resources, etc., and achieve the effects of short mixing time, sufficient mixing reaction, and improved drawing performance

Inactive Publication Date: 2018-12-21
SICHUAN FIBERGLASS GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, because basalt is formed from lava on the earth, its inherent deficiency is the fluctuation of its composition. Not only the composition of different deposits fluctuates greatly, but also the chemical composition of the same deposit has a certain fluctuation range; therefore, although the basalt on the earth is distributed Especially extensive, but there are not many basalts that can be used for stable and efficient drawing
It is relatively difficult to achieve stable and efficient wire drawing with a single type of basalt. Even if a suitable basalt mine can be selected, it will cost a lot of manpower and financial resources, and cause narrow sources of raw materials, and increase the cost of raw material transportation and collection.

Method used

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  • Basalt fiber preparation method, mineral mixture and production technology
  • Basalt fiber preparation method, mineral mixture and production technology
  • Basalt fiber preparation method, mineral mixture and production technology

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1~5、 comparative example 1~2

[0031] The batching method of basalt fiber includes: taking SiO 2 raw materials and detection of SiO 2 Content, Al 2 o 3 raw materials and detection of Al 2 o 3 content, CaO raw material and detect CaO content, MgO raw material and detect MgO content, Na 2 Feedstock for O and detection of Na 2 O content, K 2 Feedstock for O and detection of K 2 O content, Li 2 Feedstock for O and detection of Li 2 O content, Fe 2 o 3 Raw materials and detection of Fe 2 o 3 Content, ZrO 2 Raw materials and detection of ZrO 2 Content, CeO 2 raw materials and detect CeO 2 content and the raw material of MnO and detect the MnO content, counter-stirring and mixing to obtain the mineral mixture and detect the component content in the mineral mixture, and grind the mineral mixture into 200-300 mesh powder; in weight percentage, the The components in the mineral mixture are listed in Table 1.

[0032] Among them, the SiO 2 The raw material is selected from basalt, the Al 2 o 3 The...

Embodiment 6

[0040] The basalt fiber obtained by the batching method of the basalt fiber of the present invention has good performance, and the good performance of the basalt fiber obtained by the batching method of the basalt fiber of the present invention is specifically demonstrated through the following tests.

[0041] Performance test and method:

[0042] 1. Wire drawing operation temperature test

[0043] The viscosity of the basalt melt was tested with a high-temperature viscosity tester from Theta Company of the United States, and the temperature corresponding to the viscosity value of 103dPa.s was taken as the wire drawing temperature. The test results are shown in Table 2.

[0044] Table 2 Test results

[0045]

[0046]

[0047] Wherein, as can be seen from Table 2, the batching method of the basalt fiber of the present invention introduces Li 2 O, MgO, TiO 2 , ZrO 2 , CeO 2 And MnO make basalt fiber high strength, good stability, lower melting temperature, lower draw...

Embodiment 7~10

[0054] The difference between embodiment 7~10 and embodiment 1 is only:

[0055] The SiO 2 raw material, the Al 2 o 3 The raw material, the CaO raw material, the MgO raw material, the Na 2 O raw material, the K 2 The raw material of O, the Li 2 O raw material, the Fe 2 o 3 raw material, the TiO 2 The raw materials are shown in Table 4.

[0056] Table 4

[0057]

[0058]

[0059] After testing, the compounding method obtained in Examples 7-10 of the present invention uses various raw materials to hedge and mix, and the stability of the obtained basalt fiber is obviously better than that of the basalt fiber obtained by directly compounding only basalt as a single ore raw material on the market. sex. The invention adopts a variety of mineral mixtures, and the mineral mixture is prepared from various ores, so that the fluctuation range of the overall components is minimized, the stability is good, and the wire drawing performance is improved.

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Abstract

The invention discloses a basalt fiber preparation method, a mineral mixture and a production technology. The preparation method comprises the step of grinding the mineral mixture into 200 to 300-meshpowder to obtain basalt fibers. The mineral mixture is prepared from the ingredients in weight percentage: 47% to 59% of SiO2, 11% to 16% of Al2O3, 5% to 9% of CaO, 2% to 7% of MgO, 2% to 5% of Na2O,0.5 to 3% of K2O, 0 to 2.6% of Li2O, 7% to 16% of Fe2O3, 1% to 3.4% of TiO2, 0 to 3% of ZrO2, 0 to 2% of CeO2 and 0 to 2% of MnO. The used mineral mixture is prepared from varieties of ores, so thatthe whole ingredient fluctuation range is reduced to the lowest, wiredrawing performance is improved, mineral mixture ingredient contents and mutual proportional relation are controlled, strength is improved, stability is improved, elasticity modulus is improved, a melting temperature is reduced, energy is saved, glass material characteristics are changed, and improving wiredrawing performance isachieved.

Description

technical field [0001] The invention relates to the technical field of materials, in particular to a batching method of basalt fiber, a mineral mixture and a production process. Background technique [0002] Basalt fiber is made of natural basalt as raw material. After melting at a high temperature of about 1500 ℃, it is formed by a platinum-rhodium alloy bushing plate, and is continuously drawn by a wire drawing machine for tens of thousands of meters at high speed. Continuous basalt fiber is a new type of environmentally friendly inorganic fiber material, which has excellent properties such as light weight, high strength, high temperature resistance, corrosion resistance, oxidation resistance, radiation protection, heat insulation and sound insulation. It is another high-tech fiber after carbon fiber, aramid fiber and ultra-high molecular weight polyethylene fiber. It has a wide range of uses in aerospace, automobile and ship, civil engineering transportation, energy and e...

Claims

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Application Information

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IPC IPC(8): C03C13/06C03B37/00
CPCC03C13/06C03B37/00
Inventor 邹岩辉康明李军代加川罗剑超
Owner SICHUAN FIBERGLASS GRP
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