Hollow-structure biomass charcoal/TiO2 multi-wall tube/CuO photocatalyst and preparation method thereof
A technology of biomass charcoal and photocatalyst, which is applied in the direction of physical/chemical process catalysts, metal/metal oxide/metal hydroxide catalysts, chemical instruments and methods, etc., which can solve the problems of high management input and cost, secondary pollution, Harsh and other problems, to achieve the effect of no secondary pollution, low cost, efficient and fast removal
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Embodiment 1
[0033] Hollow structure biochar / TiO 2 The preparation method of multi-wall tube / CuO photocatalyst comprises the steps:
[0034] a) Wash the stalks of goosebumps with clean water, dry them and crush them with a pulverizer to keep the particle size at about 1.5 mm, then soak the stalks of goosebumps in 1mol / L acetic acid solution for 2 hours, and wash them with deionized water until neutral , dried in an oven at 100 °C for 5 h to obtain pretreated biomass.
[0035] b) Prepare a titanium isopropoxide solution according to the ratio of titanium isopropoxide: ethanol = 1:2 (volume ratio), dissolve 30 mg of pretreated biomass in 100 mL of titanium isopropoxide solution, sonicate for 20 minutes, and then dry it in a 40°C oven Dry for 4 hours to obtain titanium isopropoxide / mountain stalk.
[0036] c) Put the above-mentioned titanium isopropoxide / mountain stalk in a muffle furnace, heat up to 400°C at a rate of 5°C / min for 2 hours, and obtain a hollow structure of stalk / TiO after na...
Embodiment 2
[0040] Hollow structure biochar / TiO 2 The preparation method of multi-wall tube / CuO photocatalyst comprises the steps:
[0041] a) Wash the stalks of goosebumps with clean water, and after drying, use a pulverizer to pulverize them, keeping the particle size at about 1.5 mm, then soak the stalks of goosebumps in 2mol / L acetic acid solution for 3 hours, and wash them with deionized water until neutral , and dried in an oven at 110°C for 6h to obtain pretreated biomass.
[0042] b) Prepare a titanium isopropoxide solution according to the ratio of titanium isopropoxide: ethanol = 1:3 (volume ratio), dissolve 40 mg of pretreated biomass in 100 mL of titanium isopropoxide solution, sonicate for 30 minutes, and then heat it in an oven at 60 ° C Dry for 6h to obtain titanium isopropoxide / mountain stalk.
[0043] c) Put the above-mentioned titanium isopropoxide / goat stalk in a muffle furnace, heat up to 550°C at a rate of 7°C / min for 4 hours, and obtain a hollow structure goat stal...
Embodiment 3
[0047] Hollow structure biochar / TiO 2 The preparation method of multi-wall tube / CuO photocatalyst comprises the steps:
[0048] a) Wash the stalks of goosebumps with clean water, dry them and crush them with a pulverizer to keep the particle size at about 1.5mm, then soak the stalks of goosebumps in 3mol / L acetic acid solution for 4h, and wash them with deionized water until neutral , dried in an oven at 120°C for 8h to obtain pretreated biomass.
[0049] b) Prepare a titanium isopropoxide solution according to the ratio of titanium isopropoxide: ethanol = 1:4 (volume ratio), dissolve 50 mg of pretreated biomass in 100 mL of titanium isopropoxide solution, sonicate for 40 minutes, and then place in an oven at 80 ° C Dry for 8 hours to obtain titanium isopropoxide / mountain stalk.
[0050] c) Put the above-mentioned titanium isopropoxide / mountain stalk in a muffle furnace, heat up to 700°C at a rate of 10°C / min for 6 hours, and then naturally cool to obtain a hollow structure ...
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