Novel method for anodic oxidation of beryllium aluminum alloy

A beryllium aluminum alloy, anodic oxidation technology, applied in anodic oxidation, electrolytic coating, surface reaction electrolytic coating, etc., can solve the problems of carcinogenicity, unclear process description, increase of actual process operation cost, etc., and achieve the effect of easy industrial production

Active Publication Date: 2018-06-22
西北稀有金属材料研究院宁夏有限公司
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Problems solved by technology

The process description in the above patent applications and technical publications is not clear, and the main solvent chromic anhydride used is carcinogenic to the human body. Strict protection requirements must be followed in the actual production process, which objectively increases the operating cost of the actual process.

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  • Novel method for anodic oxidation of beryllium aluminum alloy
  • Novel method for anodic oxidation of beryllium aluminum alloy

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specific Embodiment approach

[0016] A new method of anodizing beryllium aluminum alloy, the method mainly consists of the following steps:

[0017] 1. The surface of the beryllium aluminum alloy material is processed by machining to improve the surface finish, and rinsed with deionized water repeatedly.

[0018] 2. For the beryllium aluminum alloy material that has been surface-treated in step 1, soak in an organic solution for 5-10 minutes in an air-circulating environment, and rinse with deionized water for 3 to 4 times after degreasing; The solution is: acetone, ethanol, kerosene, gasoline.

[0019] 3. The cleaned alloy material is subjected to a chemical degreasing process under certain temperature conditions, and the duration is 10-15s. The formula of chemical degreasing agent is: NaOH 10~25 g / L, Na 2 CO 3 20~30 g / L; the temperature condition of the whole degreasing process is between 40~50℃; after degreasing is finished, rinse with deionized water for 3 to 4 times.

[0020] 4. Use acidic solution to chemic...

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Abstract

The invention discloses a novel method for anodic oxidation of a beryllium aluminum alloy material, and belongs to the field of alloy materials. The method is composed of the following steps that (1),the surface of the beryllium aluminum alloy is treated in a machining manner so as to improve the surface smoothness, and then is repeatedly washed with deionized water to be clean; (2), the beryllium aluminum alloy material subjected to the surface treatment is soaked with an organic solution for 5-10 minutes to remove oil; (3), a chemical oil removal process is carried out on the beryllium aluminum alloy material, and the duration time is 10-15 seconds; (4), chemical polishing is carried out on the surface of the beryllium aluminum alloy by utilizing an acidic solution, wherein the polishing time is 10-15 seconds; (5), a proper cathode and anode area ratio is determined, a proper rack is selected to fix an anode, a proper interelectrode distance is selected to fix the positions of the two poles, and then an anodic oxidation process is started; and (6), hole sealing is carried out by adopting a potassium dichromate solution after the oxidation process is finished. According to the method, anodic oxidation is carried out on the surface of the beryllium aluminum alloy, so that the corrosion tendency of the beryllium aluminum alloy is prevented and reduced, and the corrosion resistance and the surface performance of the beryllium aluminum alloy are improved.

Description

Technical field [0001] The invention belongs to the field of surface protection of alloy materials, and particularly relates to a new method of anodic oxidation for surface protection of beryllium aluminum alloy materials. Background technique [0002] Beryllium aluminum alloy is widely used as a new aviation product due to its excellent physical properties. The user's product is used in a special environment. The moisture in the air condenses on the metal surface to make the electrolyte solution exist, which provides conditions for electrochemical corrosion. Based on the current status of enterprise aviation product research and development, in order to prevent and reduce the corrosion tendency of beryllium aluminum alloy and improve the corrosion resistance and surface performance of beryllium aluminum alloy, the experimental research on the surface protection process of beryllium aluminum alloy anodizing has very practical significance. The two phases of beryllium and aluminum...

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Application Information

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IPC IPC(8): C25D11/16C25D11/06
CPCC25D11/06C25D11/16
Inventor 谢垚李军义王东新刘兆刚饶晓芳李峰王战宏高林
Owner 西北稀有金属材料研究院宁夏有限公司
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