Finishing process of wool hat
A hat and wool technology, applied in the field of wool hats, can solve the problems that affect the wearing performance of woolen hats, cannot meet high-efficiency flame retardant performance, easily breed bacteria, etc., and achieve improved combustion performance and thermal performance, excellent flame retardant durability, Good dispersion effect
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Embodiment 1
[0022] The finishing process of a kind of wool hat that the present invention proposes comprises the following steps:
[0023] S1. Immerse the wool hat in water, ultrasonicate at 40°C for 50 minutes, and obtain a wool hat after drying;
[0024] S2. Add diethyl allyl phosphate into the emulsifier aqueous solution, emulsify at 8000r / min for 8min, add zinc oxide modified by silane coupling agent KH-570, adjust the system to be acidic, heat up to 85°C, Add benzoyl peroxide and stir evenly to obtain a mixed solution; immerse the primary-treated wool hat in S1 into the mixed solution, react at 90°C for 50 minutes, rinse and dry after the reaction to obtain a secondary-treated wool hat;
[0025] S3. Mix ethanol and acetic acid, add butyl titanate and stir evenly, then add silver fluoride and tetrabutylammonium fluoride, wash to neutral after standing at room temperature for 3 days, filter and dry to obtain material A; and arginine into water, stir evenly, add material A, soak at roo...
Embodiment 2
[0029] The finishing process of a kind of wool hat that the present invention proposes comprises the following steps:
[0030] S1. Immerse the wool hat in water, ultrasonicate at 55°C for 30 minutes, and obtain a wool hat after drying;
[0031] S2. Add diethyl allyl phosphate into the emulsifier aqueous solution, emulsify at a speed of 5000r / min for 12min, add zinc oxide modified by silane coupling agent KH-570, adjust the system to be acidic, and raise the temperature to 75°C. Add benzoyl peroxide and stir evenly to obtain a mixed solution; immerse the primary-treated wool hat in S1 into the mixed solution, react at 100°C for 30 minutes, rinse and dry after the reaction to obtain a secondary-treated wool hat;
[0032] S3. Mix ethanol and acetic acid, add butyl titanate and stir evenly, then add silver fluoride and tetrabutylammonium fluoride, place at room temperature for 2 days, wash until neutral, filter, and dry to obtain material A; Add arginine and arginine into water, ...
Embodiment 3
[0036] The finishing process of a kind of wool hat that the present invention proposes comprises the following steps:
[0037] S1. Immerse the wool hat in water, ultrasonicate at 45°C for 46 minutes, and obtain a wool hat after drying;
[0038] S2. Add diethyl allyl phosphate into the emulsifier aqueous solution, emulsify at a speed of 6000r / min for 10min, add zinc oxide modified by silane coupling agent KH-570, adjust the system to be acidic, and raise the temperature to 77°C. Add benzoyl peroxide and stir evenly to obtain a mixed solution, wherein the weight ratio of diethyl allyl phosphate, emulsifier, silane coupling agent KH-570 modified zinc oxide, and benzoyl peroxide is 50:1 : 17:1, the mass fraction of the emulsifier in the emulsifier aqueous solution is 5%; immerse the primary treatment wool hat in S1 into the mixture, react at 92°C for 45min, rinse and dry after the reaction to obtain the secondary treatment wool hat;
[0039] S3. Mix ethanol and acetic acid, add ...
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Abstract
Description
Claims
Application Information
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