Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Three-dimensional carbon fiber preform reinforced yttrium silicate composite material and preparation method thereof

A three-dimensional carbon fiber and composite material technology, applied in woven fabrics, non-woven fabrics, layered products, etc., can solve the problem of less gaseous raw materials, less than ideal deposition characteristics, and no three-dimensional carbon fiber preform reinforced yttrium silicate composite material. Research report and other problems, to achieve the effect of high densification efficiency, excellent oxidation resistance and excellent mechanical properties

Active Publication Date: 2018-01-30
NAT UNIV OF DEFENSE TECH
View PDF4 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

And for fiber-reinforced yttrium silicate composites, currently suitable for depositing Y 2 o 3 and SiO 2 The gaseous raw material is too little, and the deposition characteristics are not ideal, while the liquid raw material is relatively easy to obtain, and the performance is reliable.
So far, there is no research report on the preparation of three-dimensional carbon fiber preforms reinforced yttrium silicate composites by liquid phase method

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Three-dimensional carbon fiber preform reinforced yttrium silicate composite material and preparation method thereof
  • Three-dimensional carbon fiber preform reinforced yttrium silicate composite material and preparation method thereof
  • Three-dimensional carbon fiber preform reinforced yttrium silicate composite material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] A three-dimensional carbon fiber preform reinforced yttrium silicate composite material of the present invention, comprising a three-dimensional carbon fiber preform and yttrium silicate, wherein the yttrium silicate is a matrix, the three-dimensional carbon fiber preform is a reinforcing phase, and the yttrium silicate is uniformly filled in the three-dimensional carbon fiber In the void of the preform, the crystal phase is Y 2 Si 2 o 7 , In this implementation, the porosity of the three-dimensional carbon fiber preform reinforced yttrium silicate composite material is 12.7%.

[0048] In this embodiment, the three-dimensional carbon fiber prefabricated part is a three-dimensional carbon fiber prefabricated part obtained by stacking and sewing carbon fiber cloth, and the volume fraction of fibers in the three-dimensional carbon fiber prefabricated part is 48%.

[0049] In this example, the bending strength of the three-dimensional carbon fiber preform reinforced yttri...

Embodiment 2

[0060] A three-dimensional carbon fiber preform reinforced yttrium silicate composite material of the present invention, comprising a three-dimensional carbon fiber preform and yttrium silicate, wherein the yttrium silicate is a matrix, the three-dimensional carbon fiber preform is a reinforcing phase, and the yttrium silicate is uniformly filled in the three-dimensional carbon fiber In the void of the preform, the crystal phase is Y 2 SiO 5 , In this implementation, the porosity of the three-dimensional carbon fiber preform reinforced yttrium silicate composite material is 9.3%.

[0061] In this embodiment, the three-dimensional carbon fiber prefabricated part is a three-dimensional carbon fiber prefabricated part with a three-dimensional four-way weaving structure, and the volume fraction of fibers in the three-dimensional carbon fiber prefabricated part is 53%.

[0062] In this example, the bending strength of the three-dimensional carbon fiber preform reinforced yttrium s...

Embodiment 3

[0073] A three-dimensional carbon fiber preform reinforced yttrium silicate composite material of the present invention, comprising a three-dimensional carbon fiber preform and yttrium silicate, wherein the yttrium silicate is a matrix, the three-dimensional carbon fiber preform is a reinforcing phase, and the yttrium silicate is uniformly filled in the three-dimensional carbon fiber In the void of the preform, the crystal phase is Y 2 Si 2 o 7 and Y 2 SiO 5 Composed of mixed crystal phases, where, Y 2 Si 2 o 7 and Y 2 SiO 5 The molar ratio is 1:1. In this implementation, the porosity of the three-dimensional carbon fiber preform reinforced yttrium silicate composite material is 13.4%.

[0074] In this embodiment, the three-dimensional carbon fiber preform is a three-dimensional carbon fiber preform with a two-dimensional semi-woven structure, and the volume fraction of fibers in the three-dimensional carbon fiber preform is 46%.

[0075] In this example, the bending ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
melting pointaaaaaaaaaa
bending strengthaaaaaaaaaa
bending strengthaaaaaaaaaa
Login to View More

Abstract

The invention discloses a three-dimensional carbon fiber preform reinforced yttrium silicate composite material. The composite material comprises a three-dimensional carbon fiber preform and yttrium silicate, the yttrium silicate is a mixed crystalline phase of Y2Si2O7 and Y2SiO5, a crystalline phase of the Y2Si2O7 or a crystalline phase of the Y2SiO5, the pores of the three-dimensional carbon fiber preform are uniformly filled with the yttrium silicate, and the porosity of the three-dimensional carbon fiber preform reinforced yttrium silicate composite material is 9%-14%. A preparation methodcomprises the following steps: (1) preparing a Y2O3-SiO2 composite sol; (2) performing impregnating; (3) performing drying; (4) performing heat treatment; and (5) repeating processes including impregnating-drying-heat treatment in the steps (2)-(4). The three-dimensional carbon fiber preform reinforced yttrium silicate composite material has the advantages of low porosity, a high compact degree,high-temperature resistance, oxidation resistance, excellent mechanical properties and the like; and the preparation efficiency of the preparation method is high, and the compact degree and mechanicalproperties of the prepared composite material are remarkably improved

Description

technical field [0001] The invention relates to the technical field of high-temperature-resistant fiber-reinforced ceramic matrix composite materials, in particular to a three-dimensional carbon fiber preform reinforced yttrium silicate composite material and a preparation method thereof. Background technique [0002] Yttrium silicate is made from Y 2 o 3 and SiO 2 A material with a polycrystalline phase structure composed of three main crystal phase structures, namely Y 2 SiO 5 , Y 2 Si 2 o 7 and Y 4 Si 3 o 12 , of which the first two are the most common. In addition to being used as an optical matrix material and a dielectric material, yttrium silicate is also an excellent high-temperature resistant ceramic material, and its main crystal form Y 2 SiO 5 , Y 2 Si 2 o 7 and Y 4 Si 3 o 12 The melting points are 1980°C, 1775°C and 1950°C, respectively. While having a high melting point, yttrium silicate also has a series of excellent physical and chemical pro...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/80C04B35/16C04B35/622C04B35/624D04H1/4242D04H1/498D04C1/02D04C1/06B32B9/04
Inventor 马青松曾宽宏
Owner NAT UNIV OF DEFENSE TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com