Phosphorus-containing PBS flame-retardant material and phosphorus-containing polyurethane and preparation method
A flame retardant material, polyurethane technology, applied in the field of biodegradable flame retardant material preparation, can solve the problems of poor compatibility of PBS flame retardant modification
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[0039] Carry out the preparation of phosphorus-containing polyurethane with embodiment 1 as optimum embodiment:
[0040] Commercialized PBS resin (commercialized PBS resin in this application is purchased from Anqing Hexing Chemical Co., Ltd., injection molding grade, molecular weight Mn≈70000) is mixed with phosphorus-containing PBS flame retardant material (PPBS) by melt blending method Evenly, add the aliphatic isocyanate at the same time, slowly raise the temperature of the reaction system to 150-180°C, after the mixture is completely melted, react for 2 hours under the protection of nitrogen, and then the phosphorus-containing polyurethane can be prepared.
[0041] Table 3 shows that each component of different content obtains the different phosphorus-containing polyurethanes of series:
[0042] table 3
[0043]
[0044] Table 4 shows the test results of the phosphorus-containing polyurethanes obtained in different examples. It can be seen from the results that the pr...
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