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Preparation method of long-life amorphous hard coating layer with adjustable color transparency

A technology of hard coating and transparency, applied in the field of preparation of amorphous hard coating, can solve the problems of limited appearance and application field of coating materials, and achieve easy control of coating thickness accuracy, improved life, and controllability. strong effect

Inactive Publication Date: 2017-06-13
DONGGUAN JIAQIAN NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the currently prepared amorphous coatings are all opaque metallic luster coating materials, which limits the appearance and application fields of coating materials.

Method used

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  • Preparation method of long-life amorphous hard coating layer with adjustable color transparency

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] (1) After fully mixing cobalt, iron, thallium and boron powders with a diameter of less than 100 μm, put them into a target container, and press the surface under a pressure of 100 Mpa for 5 minutes to obtain a powder target, where the general formula of the powder target is ( CoFe) a B b Ta c , where abc is atomic percentage, and the value range is: 35≤a≤80, 15≤b≤35, 0≤c≤25.

[0027] (2) After fully mixing cobalt, iron, thallium and boron powders with a diameter of less than 100 μm, the original alloy blank is prepared by melting and casting, and the original alloy blank is subjected to 60% cold rolling deformation after hot forging. After high-temperature recrystallization heat treatment at 600°C for 2 hours, then friction stir processing at a speed of 600r / min for grain refinement, and finally low-temperature stress-relief annealing at 350°C to obtain a metal alloy target, the general formula of the metal alloy target for (CoFe) a B b Ta c , where abc is atomic...

Embodiment 2

[0030] (1) After fully mixing cobalt, iron, thallium and boron powders with a diameter of less than 100 μm, put them into a target container, and flatten the surface under a pressure of 150 Mpa for 10 minutes to obtain a powder target, where the general formula of the powder target is ( CoFe) a B b Ta c , where abc is atomic percentage, and the value range is: 35≤a≤80, 15≤b≤35, 0≤c≤25.

[0031] (2) After fully mixing cobalt, iron, thallium and boron powders with a diameter of less than 100 μm, the original alloy blank is prepared by melting and casting, and the original alloy blank is subjected to 90% cold rolling deformation after hot forging. After high-temperature recrystallization heat treatment at 800°C for 2-3h, then grain refinement by friction stir processing at a speed of 1000r / min, and finally low-temperature stress-relief annealing at 450°C, the metal alloy target is obtained, and the metal alloy target The general formula is (CoFe) a B b Ta c , where abc is a...

Embodiment 3

[0034] (1) After fully mixing cobalt, iron, thallium and boron powders with a diameter of less than 100 μm, put them into the target container, and flatten the surface under a pressure of 120 Mpa for 6 minutes to obtain a powder target, where the general formula of the powder target is ( CoFe) a B b Ta c , where abc is atomic percentage, and the value range is: 35≤a≤80, 15≤b≤35, 0≤c≤25.

[0035] (2) After fully mixing cobalt, iron, thallium and boron powders with a diameter of less than 100 μm, the original alloy billet is prepared by melting and casting, and the original alloy billet is subjected to 70% cold rolling deformation after hot forging. After high-temperature recrystallization heat treatment at 750°C for 2.5h, then friction stir processing at a speed of 800r / min for grain refinement, and finally low-temperature stress-relief annealing at 400°C to obtain a metal alloy target. The formula is (CoFe) a B b Ta c , where abc is atomic percentage, and the value range...

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Abstract

The invention provides a preparation method of an amorphous hard coating with adjustable long-life color and transparency, which comprises the following steps: after fully mixing cobalt, iron, thallium and boron powders, the surface is flattened and melted and casted respectively to obtain the powder Target material and alloy original blank; the alloy original blank is subjected to cold rolling deformation after hot forging, high temperature recrystallization heat treatment, and then friction stir processing for grain refinement, and finally low temperature stress relief annealing to obtain a metal alloy target materials, where the general formula of powder targets and metal alloy targets is (CoFe) a B b Ta c , where abc is the atomic percentage, and the value range is: 35≤a≤80, 15≤b≤35, 0≤c≤25; the powder target and the metal alloy target are placed in the multi-target magnetron sputtering In the equipment, argon and oxygen are fed, and sputtering is used to obtain an amorphous hard coating with adjustable color and transparency for a long life.

Description

technical field [0001] The invention belongs to the technical field of alloy coating materials, and in particular relates to a preparation method of an amorphous hard coating with adjustable long-life color and transparency. Background technique [0002] Amorphous metal coatings have excellent properties such as high strength, high hardness, high wear resistance, high fracture toughness, excellent corrosion resistance and high surface finish. Therefore, composite materials containing amorphous metal coatings can not only greatly Improve the intrinsic mechanical properties and corrosion resistance of the matrix material such as strength, hardness and wear resistance, prolong the service life of the matrix, and improve the surface quality of the matrix material. [0003] Chinese patent CN103065789B discloses a preparation and coating method of a high-performance iron-based amorphous metal powder core. The iron-based amorphous material is crushed into powder by ball milling, pa...

Claims

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Application Information

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IPC IPC(8): C23C14/35C23C14/06
CPCC23C14/35C23C14/067C23C14/3414
Inventor 王海燕
Owner DONGGUAN JIAQIAN NEW MATERIAL TECH CO LTD
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