Coating for liquid lifting pipe made of silicon nitride combined with silicon carbide and preparation method of coating
A silicon carbide ceramic and liquid riser technology, applied in the field of refractory materials, can solve the problems of high price, complex process, expensive materials, etc., and achieve the effects of low cost, good bonding performance and simple preparation
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Embodiment 1
[0054] This embodiment includes the following steps:
[0055] Step 1: Preparation of anti-oxidation layer:
[0056] 1) Treat the inner and outer walls of the silicon nitride bonded silicon carbide ceramic riser:
[0057] Grinding and cleaning the inner and outer walls of the silicon nitride bonded silicon carbide ceramic riser.
[0058] 2) Preparation of anti-oxidation layer slurry:
[0059] Pass silicon carbide micropowder, boron nitride, yttrium-stabilized zirconia, high alumina cement and sodium hexametaphosphate through a 200-mesh sieve respectively, then weigh 25 parts by mass of silicon carbide micropowder, 3 parts by mass of boron oxide, and 4 parts by mass of yttrium-stabilized zirconia. Parts by mass, 5 parts by mass of high alumina cement, 1 part by mass of sodium hexametaphosphate, ball milled for 2h, then add 4 parts by mass of silica sol with a mass concentration of 20%, and 40 parts by mass of aluminum dihydrogen phosphate with a mass concentration of 20%, at r...
Embodiment 2
[0072] This embodiment includes the following steps:
[0073] Step 1: Preparation of anti-oxidation layer:
[0074] 1) Treatment of the inner and outer walls of the silicon nitride bonded silicon carbide ceramic riser:
[0075] Grinding and cleaning the inner and outer walls of the silicon nitride and silicon carbide ceramic riser;
[0076] 2) Preparation of anti-oxidation layer slurry:
[0077] Pass silicon carbide micropowder, boron nitride, yttrium-stabilized zirconia, high alumina cement and sodium hexametaphosphate through a 200-mesh sieve respectively, then weigh 28 parts by mass of silicon carbide micropowder, 5 parts by mass of boron oxide, and 4 parts by mass of yttrium-stabilized zirconia. Parts by mass, 7 parts by mass of high alumina cement, 1 part by mass of sodium hexametaphosphate, ball milled for 2 hours, then added 5 parts by mass of silica sol with a mass concentration of 30%, and 45 parts by mass of aluminum dihydrogen phosphate with a mass concentration o...
Embodiment 3
[0090] This embodiment includes the following steps:
[0091] Step 1: Preparation of anti-oxidation layer:
[0092] 1) Treatment of the inner and outer walls of the silicon nitride bonded silicon carbide ceramic riser:
[0093] Grinding and cleaning the inner and outer walls of the silicon nitride and silicon carbide ceramic riser;
[0094] 2) Preparation of anti-oxidation layer slurry:
[0095] Pass silicon carbide micropowder, boron nitride, yttrium-stabilized zirconia, high alumina cement and sodium hexametaphosphate through a 200-mesh sieve respectively, then weigh 33 parts by mass of silicon carbide micropowder, 6 parts by mass of boron oxide, and 6 parts by mass of yttrium-stabilized zirconia. Parts by mass, 9 parts by mass of high alumina cement, 2 parts by mass of sodium hexametaphosphate, ball milled for 3h, then added 7 parts by mass of silica sol with a mass concentration of 50%, 50 parts by mass of aluminum dihydrogen phosphate with a mass concentration of 50%, a...
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