A method for aluminum gettering of ingot polycrystalline silicon wafer
A technology of polycrystalline silicon wafers and ingots, which is applied in the field of gettering process of ingot polycrystalline silicon wafers, can solve the problems of high carrier recombination activity, limiting the electrical properties of solar cells, etc., and achieve efficiency improvement, high industrial production value, and high stability sexual effect
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Embodiment 1
[0025] A method for aluminum gettering of cast polycrystalline silicon wafers, the specific process flow is as follows:
[0026] (1) Cleaning: The sample material is cast P-type polysilicon wafers, and the standard RCA solution cleaning method is used for cleaning: use No. Liquid HPM was ultrasonicated in a water bath at 80°C for 10 minutes to remove metal impurities;
[0027] (2) Vacuum evaporation aluminum layer: put the cleaned polysilicon wafer into the vacuum evaporation equipment, and vacuum the equipment to 7.5×10 4 Pa, aluminum is evaporated on the surface of the polycrystalline silicon wafer, and the thickness of the aluminum layer is 1.3 μm;
[0028] (3) Into the furnace: put the aluminized polysilicon wafer and the quartz boat together into the tubular annealing furnace, rush into the argon atmosphere, avoid pollution during the whole process, and raise the temperature of the tubular annealing furnace to 810°C at a uniform speed , the heating rate is 5°C / min;
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Embodiment 2
[0036] A method for aluminum gettering of cast polycrystalline silicon wafers, the specific process flow is as follows:
[0037] (1) Cleaning: The sample material is cast P-type polysilicon wafers, and the standard RCA solution cleaning method is used for cleaning: use No. Liquid HPM was ultrasonicated in a water bath at 80°C for 10 minutes to remove metal impurities;
[0038] (2) Vacuum evaporation aluminum layer: put the cleaned polysilicon wafer into the vacuum evaporation equipment, and vacuum the equipment to 7.5×10 4 Pa, aluminum is evaporated on the surface of the polycrystalline silicon wafer, and the thickness of the aluminum layer is 1.5 μm;
[0039] (3) Into the furnace: Put the aluminum-coated polycrystalline silicon wafer and the quartz boat together into the tubular annealing furnace, rush into the argon atmosphere, avoid pollution during the whole process, and raise the temperature of the tubular annealing furnace to 830°C at a uniform speed , the heating rate...
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