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High-content stable prinsepia utilis royle oil microemulsion and preparation method thereof

A green thorn fruit oil and a stable technology, which is applied in the field of high-content stable green thorn fruit oil microemulsion and its preparation field, can solve the problems of the green thorn fruit oil being insoluble in water-based systems and the like, and achieve good centrifugal stability and storage. Stability, effects of improving stability and solubility

Active Publication Date: 2016-10-19
SHAANXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The object of the present invention is to provide a high-content stable thorn fruit oil microemulsion and its preparation method. The thorn fruit oil microemulsion can effectively solve the problem that thorn fruit oil is difficult to dissolve in an aqueous system, and the preparation method is simple and easy , suitable for industrial production

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Step 1: In terms of parts by mass, take 7 parts of Tween 65, 2 parts of Span 80, 6 parts of dioctyl sodium sulfosuccinate, 3 parts of polyethylene glycol monoricinoleate, and coconut oil 8 parts of amidopropyl betaine, 5 parts of glycerin, 4 parts of n-butanol, the above-mentioned various components are first stirred at room temperature, the stirring speed is 500rpm, and the stirring time is 10min;

[0027] Step 2: In terms of parts by mass, add 20 parts of green thorn fruit oil to the mixture in step 1, and then keep the rotation speed constant and stir for 5 minutes to form the mixture A;

[0028] Step 3: In terms of parts by mass, take 0.3 parts of preservative and 160 parts of deionized water, dissolve the preservative in deionized water, which is mixture B; the preservative is 0.1 part of potassium sorbate, 0.1 part of sodium benzoate and 0.1 part of a mixture of sodium lactate;

[0029] Step 4: Slowly pour the mixture B into the mixture A in step 2 at room temper...

Embodiment 2

[0031] Step 1: In terms of parts by mass, take 3 parts of Tween 65, 7 parts of Span 80, 2 parts of dioctyl sodium sulfosuccinate, 7 parts of polyethylene glycol monoricinoleate, and coconut oil 4 parts of amidopropyl betaine, 12 parts of glycerin, 2 parts of n-butanol, the above-mentioned various components are first stirred at room temperature, the stirring speed is 300rpm, and the stirring time is 20min;

[0032] Step 2: In terms of parts by mass, add 10 parts of green thorn fruit oil to the mixture in step 1, and then keep the rotation speed constant and stir for 10 minutes to form a mixture A;

[0033] Step 3: In terms of parts by mass, take 0.1 part of preservative and 130 parts of deionized water, and dissolve the preservative in deionized water to form mixture B; the preservative used is sodium benzoate;

[0034] Step 4: Slowly pour the mixture B into the mixture A in step 2 at room temperature, and stir while pouring, the stirring speed is 300rpm, until all the mixture...

Embodiment 3

[0037] Step 1: In terms of parts by mass, take 6 parts of Tween 65, 3 parts of Span 80, 5 parts of dioctyl sodium sulfosuccinate, 4 parts of polyethylene glycol monoricinoleate, and coconut oil 5 parts of amidopropyl betaine, 10 parts of glycerin, 4 parts of n-butanol, the above-mentioned various components are first stirred at room temperature, the stirring speed is 500rpm, and the stirring time is 10min;

[0038] Step 2: In terms of parts by mass, add 12 parts of green thorn fruit oil to the mixture in step 1, and then keep the rotation speed constant and stir for 5 minutes to form a mixture A;

[0039] Step 3: In terms of parts by mass, take 0.2 parts of preservative and 140 parts of deionized water, and dissolve the preservative in deionized water to form a mixture B; the preservatives are 0.1 part of sodium lactate and 0.1 part of sodium benzoate;

[0040] Step 4: Slowly pour the mixture B into the mixture A in step 2 at room temperature, and stir while pouring, the stirr...

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PUM

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Abstract

The invention discloses high-content stable prinsepia utilis royle oil microemulsion and a preparation method thereof, and belongs to the technical field of oil microemulsification. The prinsepia utilis royle oil microemulsion is prepared from 10-20 parts of prinsepia utilis royle oil, 3-7 parts of tween-65, 2-7 parts of span-80, 2-6 parts of sodium diethylhexyl sulfosuccinate, 3-7 parts of carboxymethyl-beta-cyclodextrin, 4-8 parts of cocamidopropyl betaine, 5-12 parts of glycerin, 2-4 parts of n-butyl alcohol, 0.1-0.3 part of a preservative and 130-160 parts of deionized water. The preparation method of the prinsepia utilis royle oil microemulsion comprises the steps of mixing, stirring, shearing and the like. The prepared prinsepia utilis royle oil microemulsion has the advantages of being small in particle size, good in storage stability property and excellent in dissolving property.

Description

technical field [0001] The invention belongs to the technical field of oil micro-emulsion, and in particular relates to a high-content stable thorn fruit oil micro-emulsion and a preparation method thereof. Background technique [0002] The fatty acid composition of green thorn fruit oil is mainly unsaturated fatty acids - oleic acid and linoleic acid, of which the content of oleic acid is 33.38%, the content of linoleic acid is 40.82%; in addition, it also contains 17.2% palmitic acid and 6% Stearic acid, and contains vitamin A, vitamin D, vitamin E and vitamin K and other vitamins, every 100g green thorn fruit oil contains 3.5mg vitamin A, 2.1mg vitamin D, 11.2mg vitamin E and 0.30mg vitamin K, It is also very rich in calcium, sulfur, manganese, magnesium, potassium, phosphorus, zinc and iron and other macro and trace elements. Compared with other edible oils, the element with the highest content is potassium, with a content of 9.8mg / kg. Compared with other vegetable oils...

Claims

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Application Information

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IPC IPC(8): A61K8/92A61K8/06A61K8/49A61K8/46A61K8/44A61K8/34A61K8/60A61K8/365A61K8/36A61K8/368A61Q19/00A61K36/73A61K9/107A61P17/02
CPCA61K8/068A61K8/34A61K8/345A61K8/36A61K8/365A61K8/368A61K8/442A61K8/466A61K8/4973A61K8/4993A61K8/60A61K8/922A61K9/1075A61K36/73A61Q19/00
Inventor 刘宁李骋李超
Owner SHAANXI UNIV OF SCI & TECH
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