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Fruit, vegetable and cyclodextrin supermolecule micro-powder, method for preparing same and application of fruit, vegetable and cyclodextrin supermolecule micro-powder

A cyclodextrin and supramolecular technology, which is applied in the field of fruit and vegetable-cyclodextrin supramolecular micropowder and its preparation, can solve the problems of reducing the effect of cyclodextrin, improper timing of cyclodextrin addition, and failure to achieve protection. Achieve good fluidity and dispersion and dissolution properties, protect unstable components, and timely inclusion effects

Inactive Publication Date: 2016-06-15
江苏仙巨生物技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In the existing published technology, the technical characteristics of cyclodextrin applied to fruits and vegetables are as follows: first, cyclodextrin is used with various additives at the same time, and cyclodextrin is expected to play the role of taste masking and solubilization, while ignoring the effect of shared additives on The interference of cyclodextrin's inclusion performance not only reduces the effect of cyclodextrin, but also leads to complicated prescriptions and cumbersome technological processes, which is not worth the loss; the second is that the timing of adding cyclodextrin is improper. After pulverization, the ingredients are separated from the protection of the cells and exposed to the environment. Under the influence of light, heat, air, and water vapor, the ingredients will undergo changes such as oxidation, decomposition, taste change, and discoloration. This change is more obvious in the case of ultrafine grinding, so subsequent processing And during use, micropowder is more prone to form changes such as agglomeration, volatilization, precipitation, foaming, delamination, and coking than ordinary pulverized products
Adding cyclodextrin after crushing fruits and vegetables will fail to protect unstable components in time and prevent adverse effects such as decomposition, discoloration and odor, and the interference of other additives will not be able to fully improve the solubility of the product by cyclodextrin

Method used

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  • Fruit, vegetable and cyclodextrin supermolecule micro-powder, method for preparing same and application of fruit, vegetable and cyclodextrin supermolecule micro-powder
  • Fruit, vegetable and cyclodextrin supermolecule micro-powder, method for preparing same and application of fruit, vegetable and cyclodextrin supermolecule micro-powder
  • Fruit, vegetable and cyclodextrin supermolecule micro-powder, method for preparing same and application of fruit, vegetable and cyclodextrin supermolecule micro-powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0087] Embodiment 1. Get 20000g of fresh tomatoes and wash them, mix them with 1000g beta-CD, break them into coarse pulp with a crusher, then inject them into a colloid mill, adjust the fine grinding gear ratio to 5-15 μm, and grind them circularly for 0.5 hours to form a fine slurry. Material, 50 ℃ of vacuum dehydration in vacuum microwave drier, then room temperature vacuum drying 5 hours, pulverize, cross 100 mesh sieves to obtain 2011g bright red β-CD tomato micropowder.

[0088] Micropowder: TGA measured water content 5.16%, lycopene content 47.8mg / 100g; DTA spectrum (both measured in nitrogen atmosphere) a weak endothermic peak at 137°C after dehydration endothermic peak, no β-CD phase transition at 221°C Peak, exothermic peak at 328°C, the system is violently exothermic, ordinary tomato powder is exothermic peak at 202.85°C, and the system is violently exothermic at 336°C.

[0089] Instant tomato powder: Take 1000g of the above-mentioned fine powder, mix it with 120g o...

Embodiment 2

[0091] Embodiment 2. Take 3000g of fresh tomato and wash it, mix it with 100g α-CD, break it into a coarse slurry with a crusher, then pour it into a colloid mill, adjust the grinding gear ratio to 5-15 μm and grind it circularly for 0.5 hours, and after it becomes a fine slurry, come out Material, 50 ℃ of vacuum dehydration in vacuum microwave drier, then room temperature vacuum drying 5 hours, pulverize, cross 100 mesh sieves to obtain 248g bright red α-CD tomato micropowder.

[0092] Micropowder: Water content 6.61% as determined by TGA, lycopene content 183.2mg / 100g; DTA spectrum has no α-CD phase transition peak at 141°C after dehydration endothermic peak, and exothermic peak at 312°C.

Embodiment 3

[0093] Embodiment 3. Get 21000g of fresh day lily and wash, boil in water for 0.5 hours, mix with 3000gβ-CD and 2000ml water after draining the water, break into fine cubes with a crusher, then pour into a colloid mill, adjust the grinding gear ratio to 5- 15 μm circular grinding for 0.5 hours, after becoming a fine slurry, discharging, dewatering in a vacuum microwave dryer at 50°C under reduced pressure, then vacuum drying at room temperature for 5 hours, passing through a 100-mesh sieve to obtain 5770g of yellow β-CD day lily powder.

[0094] Micropowder: The water content is 8.33% by TGA; after the dehydration endothermic peak of the DTA spectrum (combined), a broad endothermic peak appears at 155°C, and the β-CD phase transition peak at 221°C disappears. The heat peak disappeared, and only a weak exotherm appeared at 338.90°C.

[0095] Instant daylily powder: Take 1000g of micropowder, mix it with 100g of lactitol, granulate with a little water, pass through a 40-mesh sie...

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Abstract

The invention discloses fruit, vegetable and cyclodextrin supermolecule micro-powder, a method for preparing the same and application of the fruit, vegetable and cyclodextrin supermolecule micro-powder.The fruit, vegetable and cyclodextrin supermolecule micro-powder is mainly made of cyclodextrin, fruits and vegetables.Compared with the prior art, the fruit, vegetable and cyclodextrin supermolecule micro-powder, the method and the application have the advantages that technical difficult problems in the aspect of micronizing fruits and vegetables can be solved by the aid of the simple technological method, the original contents of components of the fresh fruits and the fresh vegetables can be kept to the greatest extent, degradation of macromolecules can be promoted, the contents of water-soluble small-molecular components can be increased, and products have high nutritional available value; the dispersibility and the solubility of the fruits and the vegetables can be improved, nutrition absorption and utilization can be enhanced, and the fruit, vegetable and cyclodextrin supermolecule micro-powder has excellent taste and is low in dose and high in compliance; optional chemical reagents or solvents are omitted in preparation procedures, and accordingly the fruit, vegetable and cyclodextrin supermolecule micro-powder is high in safety; the products are good in flowability, follow-up preparation processing can be facilitated, and the fruit, vegetable and cyclodextrin supermolecule micro-powder is excellent in performance and has fine and uniform particle sizes; the powdery products and preparations are good in stability, long in shelf life and easy to carry, store and transport; the technical method is simple and is free of emission or pollution, and accordingly the fruit, vegetable and the cyclodextrin supermolecule micro-powder, the method and the application conform to the 'efficient, high-quality and environment-friendly' development direction of the food processing industry.

Description

technical field [0001] The invention relates to a fruit and vegetable-cyclodextrin supramolecular micropowder and its preparation method and application, belonging to the technical field of food. Background technique [0002] Fruits and vegetables are an important source of nutrients that people need daily. Their seasonality, high water content and perishable properties make dried fruits and vegetables a new trend in product development. Fruits and vegetables include fresh fruits and vegetables and their nuts or roots. Fruits and vegetables are directly processed into dehydrated fruits and vegetables, fruit and vegetable powder and nuts fried seeds are the main product forms of dried fruits and vegetables at present. Dried fruits and vegetables have a long shelf life, high utilization rate, It has many advantages such as rich nutrition, convenient use, easy transportation and storage, and thus has a huge market. [0003] Fruits and vegetables contain a large amount of nutri...

Claims

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Application Information

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IPC IPC(8): A23L19/00A23L29/30A23L25/00
CPCA23V2002/00A23V2250/5112
Inventor 任勇郭廷华李仁靓鲁辉
Owner 江苏仙巨生物技术有限公司
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