Preparation method of decoquinate
A technology of decoquinate and sodium hydroxide, which is applied in the field of poultry medicine preparation technology, can solve the problems of high reaction temperature, high equipment requirements, and easy spraying of materials, and achieve high selectivity, short process route, and no corrosion The effect of the device
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[0019] In order to make the objects and advantages of the present invention clearer, the present invention will be further described in detail below in conjunction with the examples. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.
[0020] Such as figure 1 As shown, the embodiment of the present invention provides a preparation method of decoquinate, comprising the following steps:
[0021] S1, diazotization
[0022] Put 7.5 parts of aniline and 22 parts of water into the reaction kettle, cool down to 0°C, stir slowly, add 21 parts of 30-32% concentrated hydrochloric acid, after the addition is completed, the temperature drops to 0°C, and then add sodium nitrite solution (5.9 part, 22 parts of water), after the flow addition is completed, continue to react at this temperature for 1h to obtain the diazonium salt solution of aniline, which is kept at low temperature for sub...
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