Glutathione-Au/Ag alloy nano material, preparation method and application thereof
A glutathione, gold-silver alloy technology, applied in nanotechnology, luminescent materials, nanotechnology and other directions, can solve the problems of complex process, unenvironmental protection, difficult control of stability and uniformity, etc., to achieve stable and uniform structure, avoid The effect of simple and convenient use and preparation of toxic reagents
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Embodiment 1
[0048]The preparation method of glutathione-gold-silver alloy nanomaterial is as figure 1 shown, including the following steps:
[0049] Step 1: Add 2.5 mL of 100 mM silver nitrate solution and 2.5 mL of 100 mM trisodium citrate solution into 39 mL of deionized water and stir evenly.
[0050] Step 2: Add 6 mL, 50 mM freshly prepared sodium borohydride solution into the mixed solution in Step 1, and stir continuously for 14 hours to obtain a silver nanoparticle solution.
[0051] Step 3: Add 307.3 mg of glutathione powder into the silver nanoparticle solution obtained in step 2, then react the mixture in an oil bath for 50 hours at 70° C. to obtain a light orange solution, which is stabilized with glutathione solution of silver nanoparticles.
[0052] Step 4, add 4 mL of the glutathione-stabilized silver nanoparticle solution of step 3 into 10.8 mL of deionized water, and stir evenly; then slowly add 1.2 mL, 10 mM chloroauric acid solution (HAuCl 4 4H 2 O), continue to stir...
Embodiment 2
[0056] The preparation method of glutathione-gold-silver alloy nanomaterial is as figure 1 shown, including the following steps:
[0057] Step 1: Add 2.64 mL of 100 mM silver nitrate solution and 2.64 mL of 100 mM trisodium citrate solution into 41.25 mL of deionized water and stir evenly.
[0058] Step 2: Add 7.93mL, 50mM freshly prepared sodium borohydride solution into the mixed solution in step 1, and keep stirring for 12h. After stirring overnight, a silver nanoparticle solution was obtained.
[0059] Step 3, 307.3 mg of glutathione powder is added to the silver nanoparticle solution obtained in step 2, and then the mixture is reacted in an oil bath for 40 hours at 65° C. to obtain a light orange solution, which is stabilized with glutathione Silver nanoparticles solution.
[0060] Step 4, add 4 mL of the glutathione-stabilized silver nanoparticle solution of step 3 into 10.8 mL of deionized water, and stir evenly; then slowly add 1.2 mL, 10 mM chloroauric acid solutio...
Embodiment 3
[0064] The glutathione-gold-silver alloy nanomaterials prepared according to the methods of Example 1 and Example 2 were characterized by TEM, fluorescence, infrared, ultraviolet, XRD and SEM.
[0065] Such as figure 2 The three-dimensional fluorescence map of the glutathione-gold-silver alloy nanomaterial shown. It can be seen from the figure that the gold-silver alloy fluorescent nanomaterial prepared by the present invention has relatively strong fluorescence characteristics.
[0066] Such as image 3 and Figure 4 The TEM image and particle size distribution diagram of the glutathione-gold-silver alloy nanomaterials shown, in the case of glutathione as a stabilizer and surface protection agent, the gold-silver alloy nanomaterials are uniformly and stably distributed, and the particle size The diameter distribution is uniform, and the size is about 28.5nm.
[0067] Such as Figure 5 The optimal relationship diagram of fluorescence intensity of glutathione-gold-silver ...
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