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Method for improving magnetic property of sintered neodymium-iron-boron permanent magnet

A permanent magnet and NdFeB technology, which is applied in the field of improving the magnetic properties of sintered NdFeB permanent magnets, can solve the problem that the Nd-rich phase cannot form magnetic isolation, the thin layer of the Nd-rich phase is not uniform and continuous, and the main phase grains of the magnet are weak. Sharp corners and other problems can be solved, and the effects of good application prospects, microstructure optimization, remanence and maximum energy product improvement can be achieved.

Active Publication Date: 2015-07-08
NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are two problems with this method: (1) the addition of heavy rare earths will reduce the remanence of permanent magnets; (2) the resources of heavy rare earths are scarce and the production cost is high
However, after the existing heat treatment technology, there are still problems such as sharp corners and defects in the main phase grains in the magnet, and the Nd-rich phase thin layer wrapped outside the main phase grains is not uniform and continuous, resulting in the failure of the Nd-rich phase to form. Very good magnetic isolation, so the magnet coercive force is low

Method used

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  • Method for improving magnetic property of sintered neodymium-iron-boron permanent magnet
  • Method for improving magnetic property of sintered neodymium-iron-boron permanent magnet
  • Method for improving magnetic property of sintered neodymium-iron-boron permanent magnet

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Experimental program
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Effect test

Embodiment 1

[0026] In this embodiment, induction heating is used to improve the magnetic properties of sintered NdFeB magnets, and the specific process steps are:

[0027] 1) Process the Nd-Fe-B magnet after high-temperature sintering and tempering at 500°C for 2 hours into a cylindrical shape. The diameter of the cylinder is about 10mm, and the height is about 10mm. The surface is polished with sandpaper and cleaned.

[0028] 2) Test the magnetic properties of the magnet after step 1) using the NIM-500C permanent magnet material high temperature measurement system at room temperature, and obtain the demagnetization curve of the magnet before induction heating treatment, see figure 1 . The magnetic performance parameters are shown in Table 1.

[0029] 3) Put the magnet tested in step 2) into the quartz crucible of the vacuum induction furnace, and evacuate the furnace chamber so that the air pressure is as low as 1.4×10 -2 Pa, then pass Ar gas to clean the furnace cavity twice, and the...

Embodiment 2

[0034] In this example, induction heating is used to improve the magnetic properties of sintered NdFeB magnets. The specific process steps are basically the same as in Example 1, the difference is that in step 4), the temperature of the magnet is raised to 780°C after induction heating Temperature insulation, insulation time is 30 minutes.

Embodiment 3

[0036] In this embodiment, induction heating is used to improve the magnetic properties of sintered NdFeB magnets. The specific process steps are basically the same as in Embodiment 1, the difference is that the furnace cavity of the vacuum induction furnace in step 3) is vacuum, and the air pressure is lower than 7.8×10 -3 Pa; in step 4), the temperature of the magnet is raised to 700°C after induction heating and then kept at this temperature for 30 minutes.

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Abstract

Provided is a method for improving the magnetic performance of a sintered neodymium-iron-boron permanent magnet. According to the method, a sintered magnet undergoes inductive eddy current heating to turn a neodymium-rich phase thereof into a liquid phase, thus on the one hand, under the effect of an induced electromagnetic field, the flow of the neodymium-rich liquid phase can be intensified through electromagnetic stirring of induced eddy currents, so as to optimize the microstructure of the magnet; and on the other hand, main phase grains are more prone to rotate along the magnetic field direction of an induction coil, further increasing the degree of orientation of the magnet. Experiments prove that the coercive force of the sintered neodymium-iron-boron permanent magnet is somewhat improved, so does the squareness thereof. And meanwhile, both the remanence and the maximum magnetic energy product of the permanent magnet are also boosted. In addition, the method has the advantages of cleanliness without any pollution, high energy efficiency, great simplicity and practicability and so forth, and accordingly is highly promising in application.

Description

technical field [0001] The invention relates to the technical field of NdFeB permanent magnets, and relates to a method for improving the magnetic properties of sintered NdFeB permanent magnets. Background technique [0002] Rare earth permanent magnet materials, as a functional material with important influence, have been widely used in energy, transportation, communication, machinery, medical, computer, home appliances, and national defense technology and other fields, and have penetrated into all aspects of the national economy and people's livelihood. The dosage has become one of the important symbols to measure the country's comprehensive national strength and the level of national economic development. At present, my country has become the world's largest production base of rare earth permanent magnets, and it is also an important application market. [0003] In the 1980s, the intermetallic compound Nd 2 Fe 14 The third generation of permanent magnet materials based...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F41/02
CPCB22F2998/10B22F2999/00C21D1/42C22C38/00C22C38/002C22C38/005C22C2202/02H01F1/0577Y02P10/25B22F3/10B22F2003/248B22F2202/07B22F2202/05
Inventor 陈岭郭帅闫阿儒陈仁杰严长江丁广飞
Owner NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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