Preparation method for high-dispersity carbon fiber
A high-dispersibility, carbon fiber technology, applied in the direction of fiber chemical characteristics, textiles and papermaking, rayon chemical post-treatment, etc., can solve the problems of low strength, poor carbon fiber dispersibility, etc., to promote wettability, improve dispersibility, The effect of shortening the time
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Embodiment 1
[0027] A kind of preparation method of highly dispersible carbon fiber in the present embodiment, it comprises the following steps:
[0028] 1) Oiling and bundling: During the melt-spinning process of pitch carbon fiber precursors, spinning oil tankers are used to integrate the precursors into 48K fiber bundles with inorganic solid particle clustering oils. The oiling rate of inorganic solid particle clustering oils is asphalt 1.5% of the weight of carbon fiber precursor;
[0029] 2) chopping: cutting the oiled fiber bundles into 120mm chopped strands;
[0030] 3) Pre-melting treatment: Treat the chopped strands with hot air at a temperature of 250°C and a wind speed of 10m / s for 1h;
[0031] 4) Spray wetting and penetrating agent: mix high-temperature-resistant fluorocarbon surfactant, water-soluble silicone oil and water to prepare a penetrating agent with a surface tension of 35 dyn / cm, and use the penetrating agent to treat the chopped strands after pre-infusion treatment...
Embodiment 2
[0037] A kind of preparation method of highly dispersible carbon fiber in the present embodiment, it comprises the following steps:
[0038] 1) Oiling and bundling: During the melt-spinning process of pitch carbon fiber precursors, spinning oil tankers are used to integrate the precursors into 10K fiber bundles with inorganic solid particle clustering oils. The oiling rate of inorganic solid particle clustering oils is asphalt 1.0% by weight of carbon fiber precursor;
[0039] 2) chopping: cutting the oiled fiber bundles into 8mm chopped strands;
[0040] 3) Pre-melting treatment: Treat the chopped strands with hot air at a temperature of 180°C and a wind speed of 6m / s for 0.8h;
[0041] 4) Spray wetting and penetrating agent: mix high-temperature-resistant fluorocarbon surfactant, water-soluble silicone oil and water to prepare a penetrating agent with a surface tension of 25 dyn / cm, and use the penetrating agent to treat the chopped strands after pre-infusion treatment. Sp...
Embodiment 3
[0047] A kind of preparation method of highly dispersible carbon fiber in the present embodiment, it comprises the following steps:
[0048] 1) Oiling and bundling: During the melt-spinning process of pitch carbon fiber precursors, spinning oil tankers are used to integrate the precursors into 1K fiber bundles with inorganic solid particle clustering oils. The oiling rate of inorganic solid particle clustering oils is asphalt 0.1% of the weight of carbon fiber precursor;
[0049] 2) chopping: cutting the oiled fiber bundles into 2mm chopped strands;
[0050] 3) Pre-melting treatment: Treat the chopped strands with hot air at a temperature of 100°C and a wind speed of 1m / s for 0.5h;
[0051] 4) Spray wetting and penetrating agent: mix high-temperature-resistant fluorocarbon surfactant, water-soluble silicone oil and water to prepare a penetrating agent with a surface tension of 10 dyn / cm, and use the penetrating agent to treat the chopped strands after pre-infusion treatment. S...
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