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A kind of preparation technology and device of vitamin D3 microcapsule powder

A technology of microcapsule powder and preparation process, which is applied in the direction of microcapsules, capsule delivery, medical preparations of non-active ingredients, etc., which can solve problems such as poor fluidity, uneven product particles, waste of resources, etc., and improve water solubility and palatability, avoiding excessive powder spraying temperature, and increasing granulation speed

Active Publication Date: 2017-03-01
豆源和(山东)食品饮料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the selection of microcapsule coating materials, leather gelatin or animal gelatin is mostly used in traditional techniques. Although coating can also be completed to a certain extent, and the cost is relatively low, leather gelatin and animal gelatin often contain more Harmful substances such as cadmium, arsenic, and aflatoxin have been unable to meet the current product safety and hygiene standards
In addition, gelatin-coated products have poor fluidity and poor water solubility, especially not conducive to cold water diffusion and poor release, which greatly affects the use effect of the product
[0003] In addition, granulation spray is a commonly used technical method. Spray granulation inevitably involves product coating. The quality of the coating effect mainly depends on the coating material and drying technology. How to disperse the material particles as homogeneously as possible , complete heat and mass transfer in an instant, avoid material sticking or sticking to the wall, and complete drying is a technical problem faced in this field. The combination of spraying and drying technology in the traditional process is relatively simple, resulting in product coating. The stability is poor, and the product particles are not uniform enough
At present, most of the production equipment of vitamin D3 microcapsule powder is unreasonable due to the unreasonable structural design, so that the vitamin D3 microcapsule powder cannot be fully dried during the production process, resulting in defects such as uneven particle size and sticky particles, which affect the product. The quality and efficiency of continuous production, it is difficult to achieve effective recycling of coating components scattered in granulation, sieving, drying and other processes, resulting in a large waste of resources

Method used

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  • A kind of preparation technology and device of vitamin D3 microcapsule powder
  • A kind of preparation technology and device of vitamin D3 microcapsule powder
  • A kind of preparation technology and device of vitamin D3 microcapsule powder

Examples

Experimental program
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Effect test

Embodiment 1

[0033] Embodiment 1: Preparation of vitamin D3 microcapsule powder:

[0034] (1) Add BHT and VD3 oil to sunflower oil, and drain the oil after completely dissolving at a temperature of 40°C. The oil drain pipe is filtered with a 120-mesh stainless steel screen. The weight ratio of BHT, VD3 oil, and sunflower oil to BHT: VD3 oil: sunflower oil is 0.001:0.5:1.

[0035] (2) Add purified water into the emulsification tank, the ratio of purified water to VD3 oil by weight is 1:4.0, while the jacket is heating up, the ratio of modified starch: maltodextrin: white sugar: VD3 oil is 0.4:4.0:0.5:1 Ratio in parts by weight, feed modified starch, maltodextrin, white sugar, stir to dissolve completely, control the temperature at 50°C, add the VD3 oil mixture to the emulsification kettle, the temperature in the emulsification kettle is 65°C, measure the viscosity, and control it at 30-60 For centipoise, the temperature is controlled at 65°C during the measurement, the emulsion is circulat...

Embodiment 2

[0040] Embodiment 2: Preparation of vitamin D3 microcapsule powder:

[0041] (1) Add BHT and VD3 oil to corn oil, and drain the oil after completely dissolving at a temperature of 50°C. The oil drain pipe is filtered with a 120-mesh stainless steel screen. The weight ratio of BHT, VD3 oil, and corn oil is BHT:VD3 oil : Corn oil is 0.01:5:5.

[0042] (2) Add purified water into the emulsification tank, the ratio of purified water to VD3 oil is 1:5.0, and the ratio of modified starch: maltodextrin: white sugar: VD3 oil is 1: 6.0:1.5:1, feed modified starch, maltodextrin, white sugar, stir to dissolve completely, control the temperature at 60°C, put the VD3 oil mixture into the emulsification kettle, the temperature in the emulsification kettle is 75°C, measure the viscosity, and control it at 30-60 For centipoise, the temperature is controlled at 68°C during the measurement, the emulsion is circulated for 130 minutes, and the viscosity is re-measured after the reflux is complet...

Embodiment 3

[0047] Embodiment 3: Preparation of vitamin D3 microcapsule powder:

[0048] (1) Add BHT and VD3 oil to sunflower oil, and drain the oil after completely dissolving at a temperature of 45°C. The oil drain pipe is filtered with a 120-mesh stainless steel screen. The weight ratio of BHT, VD3 oil, and sunflower oil to BHT: VD3 oil: sunflower oil is 0.001:2:3;

[0049] (2) Add purified water into the emulsification tank, the ratio of purified water to VD3 oil is 1:4.5, and the ratio of modified starch:maltodextrin:white sugar:VD3 oil is 0.6 while the jacket is heating up: 5.0:1:1, feed modified starch, maltodextrin, white sugar, stir to dissolve completely, control the temperature at 55°C, put the VD3 oil mixture into the emulsification kettle, the temperature in the emulsification kettle is 70°C, measure the viscosity, and control it at 30-60 For centipoise, the temperature is controlled at 66°C during the measurement, the emulsion is circulated for 120 minutes, and the viscosit...

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Abstract

The invention relates to a preparation process and a preparation device of vitamin D3 microcapsule powder. In the preparation process, VD3 oil, sunflower seed oil or corn oil, medicinal starch, maltodextrin, modified starch, white sugar, calcium phosphate and 2,6-di-t-buty-4-methylphenol (BHT) are used as main raw materials. The preparation process and the preparation device are reasonably improved and optimized, the production time is greatly shortened and the whole production process is controlled; through layer-by-layer drying and step-by-step recycling, the prepared vitamin D3 microcapsule powder has smooth and flat surface, and the safety, the fluidity, the mouth feel and the water solubility of the vitamin D3 microcapsule powder are greatly improved; the waste of resources is reduced, the continuous large-scale production is implemented, and the production cost is reduced.

Description

technical field [0001] The invention relates to the technical field of production of vitamin D3 microcapsule powder, in particular to a preparation process and device of vitamin D3 microcapsule powder. Background technique [0002] In the production process of vitamin D3 microcapsule powder, spray drying and microcapsule coating are the two most critical technical steps, which directly affect the safety, fluidity, taste and water solubility of the product. The microcapsule wall material refers to the shell material used to coat the core material during microencapsulation, also known as encapsulation material, capsule material, and shell material. Most of the materials that can be used as microcapsule wall materials are inert polymeric natural polymers, semi-synthetic polymers and synthetic polymer materials. Among them, natural polymer materials have the advantages of non-toxicity, good film-forming properties, and good stability, and are widely used, but their mechanical s...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K9/50A61K47/26A61K47/36A61K31/593A61J3/07B01J3/02
Inventor 季华
Owner 豆源和(山东)食品饮料有限公司
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