A kind of preparation technology and device of vitamin D3 microcapsule powder
A technology of microcapsule powder and preparation process, which is applied in the direction of microcapsules, capsule delivery, medical preparations of non-active ingredients, etc., which can solve problems such as poor fluidity, uneven product particles, waste of resources, etc., and improve water solubility and palatability, avoiding excessive powder spraying temperature, and increasing granulation speed
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Embodiment 1
[0033] Embodiment 1: Preparation of vitamin D3 microcapsule powder:
[0034] (1) Add BHT and VD3 oil to sunflower oil, and drain the oil after completely dissolving at a temperature of 40°C. The oil drain pipe is filtered with a 120-mesh stainless steel screen. The weight ratio of BHT, VD3 oil, and sunflower oil to BHT: VD3 oil: sunflower oil is 0.001:0.5:1.
[0035] (2) Add purified water into the emulsification tank, the ratio of purified water to VD3 oil by weight is 1:4.0, while the jacket is heating up, the ratio of modified starch: maltodextrin: white sugar: VD3 oil is 0.4:4.0:0.5:1 Ratio in parts by weight, feed modified starch, maltodextrin, white sugar, stir to dissolve completely, control the temperature at 50°C, add the VD3 oil mixture to the emulsification kettle, the temperature in the emulsification kettle is 65°C, measure the viscosity, and control it at 30-60 For centipoise, the temperature is controlled at 65°C during the measurement, the emulsion is circulat...
Embodiment 2
[0040] Embodiment 2: Preparation of vitamin D3 microcapsule powder:
[0041] (1) Add BHT and VD3 oil to corn oil, and drain the oil after completely dissolving at a temperature of 50°C. The oil drain pipe is filtered with a 120-mesh stainless steel screen. The weight ratio of BHT, VD3 oil, and corn oil is BHT:VD3 oil : Corn oil is 0.01:5:5.
[0042] (2) Add purified water into the emulsification tank, the ratio of purified water to VD3 oil is 1:5.0, and the ratio of modified starch: maltodextrin: white sugar: VD3 oil is 1: 6.0:1.5:1, feed modified starch, maltodextrin, white sugar, stir to dissolve completely, control the temperature at 60°C, put the VD3 oil mixture into the emulsification kettle, the temperature in the emulsification kettle is 75°C, measure the viscosity, and control it at 30-60 For centipoise, the temperature is controlled at 68°C during the measurement, the emulsion is circulated for 130 minutes, and the viscosity is re-measured after the reflux is complet...
Embodiment 3
[0047] Embodiment 3: Preparation of vitamin D3 microcapsule powder:
[0048] (1) Add BHT and VD3 oil to sunflower oil, and drain the oil after completely dissolving at a temperature of 45°C. The oil drain pipe is filtered with a 120-mesh stainless steel screen. The weight ratio of BHT, VD3 oil, and sunflower oil to BHT: VD3 oil: sunflower oil is 0.001:2:3;
[0049] (2) Add purified water into the emulsification tank, the ratio of purified water to VD3 oil is 1:4.5, and the ratio of modified starch:maltodextrin:white sugar:VD3 oil is 0.6 while the jacket is heating up: 5.0:1:1, feed modified starch, maltodextrin, white sugar, stir to dissolve completely, control the temperature at 55°C, put the VD3 oil mixture into the emulsification kettle, the temperature in the emulsification kettle is 70°C, measure the viscosity, and control it at 30-60 For centipoise, the temperature is controlled at 66°C during the measurement, the emulsion is circulated for 120 minutes, and the viscosit...
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