Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Composite heat insulation material using phenolic resin and perlite as major raw materials and preparation method of composite heat insulation material

A technology of composite thermal insulation material and phenolic resin, which is applied in the field of thermal insulation material and its preparation, can solve the problems of organic thermal insulation materials such as aging resistance, toxic gas discharge, and small thermal conductivity, and achieve small deformation coefficient, good fire resistance, The effect of stable performance

Inactive Publication Date: 2014-09-24
XINYANG NORMAL UNIVERSITY
View PDF1 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Organic thermal insulation material then mainly contains foamed polystyrene board, extruded polystyrene board, spray polyurethane, phenolic resin foam board etc., as the patent application that publication number is CN101565541; The thermal conductivity of organic thermal insulation material is little, and thermal insulation effect is good, but, They are easy to burn and are not suitable for places with strict fire hazard requirements. Once a fire occurs, the spread of the flame will be accelerated, and a large amount of toxic gas will be discharged.
In addition, organic thermal insulation materials are not resistant to aging, have a large deformation coefficient, poor stability, and poor safety.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Composite heat insulation material using phenolic resin and perlite as major raw materials and preparation method of composite heat insulation material

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0030] Its specific preparation method steps are as follows:

[0031] (1) Grind the solid phenolic resin to 80~100 mesh or choose powdery resin directly, and choose a bulk density of 80~150 kg / m 3 Spherical closed-cell expanded perlite bulk;

[0032] (2) According to the mass fraction of resin 20~70%, expanded perlite 30~80%, auxiliary agent 5~10% to prepare raw materials;

[0033] (3) Fully mix the raw materials in step (2) evenly, and put them into a steel mold;

[0034] (4) Under the conditions of compression ratio of 1.25-2.5 and hot-pressing temperature of 200-240°C, hot-pressing and holding pressure for 1.5-2.5 hours, a composite insulation material with phenolic resin and perlite as the main raw materials can be obtained.

Embodiment 1

[0036] (1) Grind the solid boron-modified phenolic resin to 80-100 mesh; choose a bulk density of 80-150 kg / m 3 Spherical closed-cell expanded perlite bulk; choose silicone water repellent, hexamethylenetetramine curing agent, zinc stearate lubricant, and nitrile rubber toughening agent.

[0037] (2) According to the mass fraction of resin 40%, expanded perlite 50%, additives 10% (including 1% water-repellent agent, 7% curing agent, 1% lubricant, 1% toughening agent) to prepare raw materials.

[0038] (3) Mix the raw materials thoroughly and evenly, and put them into steel molds.

[0039] (4) Under the condition of compression ratio of 1.67 and hot pressing temperature of 220 °C, hot pressing was performed, and the pressure was maintained for 2 hours to obtain a phenolic resin / perlite composite insulation material.

[0040] The obtained phenolic resin / perlite composite insulation material sample has an apparent density of 290 Kg / m 3 , thermal conductivity 0.042 W / (m﹐K), comp...

Embodiment 2

[0042] (1) Grind the solid boron-modified phenolic resin to 80-100 mesh; choose a bulk density of 80-150 kg / m 3 Spherical closed-cell expanded perlite bulk; choose silicone water repellent, hexamethylenetetramine curing agent, zinc stearate lubricant, and nitrile rubber toughening agent.

[0043] (2) According to the mass fraction of resin 40%, expanded perlite 50%, additives 10% (including 1% water-repellent agent, 7% curing agent, 1% lubricant, 1% toughening agent) to prepare raw materials.

[0044] (3) Mix the raw materials thoroughly and evenly, and put them into steel molds.

[0045] (4) Under the conditions of compression ratio of 2 and hot pressing temperature of 220 °C, hot pressing was performed, and the pressure was maintained for 2 hours to obtain a phenolic resin / perlite composite insulation material.

[0046] The obtained phenolic resin / perlite composite insulation material sample has an apparent density of 320 Kg / m 3 , thermal conductivity 0.048 W / (m﹐K), compre...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
densityaaaaaaaaaa
flexural strengthaaaaaaaaaa
flexural strengthaaaaaaaaaa
Login to View More

Abstract

The invention discloses a composite thermal insulation material with phenolic resin and expanded perlite as main raw materials and a preparation method thereof. The phenolic resin, expanded perlite and an appropriate amount of additives are evenly mixed, molded, and hot-pressed with different compression ratios. forming. The phenolic resin is boron-modified thermoplastic solid phenolic resin, the dosage is 20~70Wt%; the expanded perlite is bulk material with a bulk density of 80~150kg / m3, and the dosage is 30~80Wt%; the compression ratio is 1.25~2.5; 200~240℃, holding time 1.5~2.5h. The apparent density of the sample is 280~350Kg / m3, the thermal conductivity is 0.037~0.068W / (m﹐K), the compressive strength is 1.1~1.8MPa, the flexural strength is 0.8~1.5MPa, and the combustion performance is B1. The composite thermal insulation material of the invention has the advantages of low thermal conductivity of the organic thermal insulation material and high strength and non-combustibility of the inorganic thermal insulation material.

Description

technical field [0001] The invention relates to the field of thermal insulation materials and their preparation, in particular to a composite thermal insulation material with phenolic resin and perlite as main raw materials and a preparation method thereof Background technique [0002] Existing thermal insulation materials mainly include inorganic thermal insulation materials and organic thermal insulation materials. Inorganic thermal insulation materials mainly include perlite, vermiculite, calcium silicate, foamed cement, mineral wool, glass wool, etc. For example, the patent application with publication number CN102336561A, compared with organic thermal insulation materials, the thermal conductivity of inorganic thermal insulation materials is relatively large , the thermal insulation effect is slightly poor, but fire retardant, small deformation coefficient, anti-aging, stable performance, long service life; [0003] Organic thermal insulation material then mainly conta...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C08L61/14C08K7/26B29C51/18B29C51/46
Inventor 刘鹏陈亚丽井强山陈延东
Owner XINYANG NORMAL UNIVERSITY
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products