Antibacterial ceramic coating of non-stick pan, preparation method and non-stick pan thereof
A technology of antibacterial ceramics and non-stick pans, applied in the field of antibacterial ceramic coatings and non-stick pans, to achieve good mechanical properties, good high temperature resistance, and good thermal conductivity.
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Embodiment 1
[0025] The various raw materials used, including silver nitrate, aluminum nitrate and ethyl orthosilicate, are all analytically pure.
[0026] First dissolve 74 grams of silver nitrate, 1000 milliliters of distilled water, and 20 milliliters of nitric acid. Add 750 grams of aluminum nitrate to the solution, and then add 1200 milliliters of water to completely dissolve it to prepare a clear and transparent solution for use; weigh 840 grams of orthosilicic acid Then add 200 ml of water, 200 ml of absolute ethanol, and 5 ml of nitric acid to it. Stir thoroughly to obtain the hydrolyzed solution for use. The measured pH value is 2; the clear and transparent solution and the hydrolyzed solution are thoroughly mixed and stirred at a constant temperature. The solution was fully reacted for 3 hours at a temperature of 80°C and gelled. After the gelled colloid was placed in a constant temperature drying oven at 150°C, it was completely dried and then calcined in a muffle furnace at 1100°C ...
Embodiment 2
[0029] The raw materials used, including silver nitrate, aluminum nitrate and ethyl orthosilicate, are all analytically pure.
[0030] First dissolve 80 grams of silver nitrate, 1000 milliliters of distilled water, and 20 milliliters of nitric acid. Add 800 grams of aluminum nitrate to the solution, and then add 1200 milliliters of water to completely dissolve it to prepare a clear and transparent solution for later use; weigh 1000 grams of orthosilicic acid Then add 400 ml of water, 400 ml of absolute ethanol, and 7 ml of nitric acid to it. After stirring thoroughly, the hydrolyzed solution is obtained for use. The measured pH value is 1.8; the clear and transparent solution and the hydrolyzed solution are thoroughly mixed, and the The solution was fully reacted and gelled at a temperature of 70°C with a stirrer for 3 hours. After the gelled colloid was placed in a constant temperature drying oven at 200°C, it was completely dried and then calcined in a muffle furnace at 1200°C f...
Embodiment 3
[0033] First dissolve 100 grams of silver nitrate, 1000 milliliters of distilled water, and 20 milliliters of nitric acid. Add 900 grams of aluminum nitrate to the solution, and then add 800 milliliters of water to completely dissolve it to prepare a clear and transparent solution for later use; weigh 1000 grams of orthosilicic acid Then add 300 ml of water, 300 ml of absolute ethanol, and 7 ml of nitric acid to it. After stirring thoroughly, the hydrolyzed solution is obtained for use. The measured pH value is 1.6; the clear and transparent solution and the hydrolyzed solution are thoroughly mixed, and the The solution was fully reacted with a stirrer at 90°C for 2 hours and gelled. After the gelled colloid was placed in a constant temperature drying oven at 180°C for thorough drying, it was calcined in a muffle furnace at 1150°C for 3 hours to synthesize.
[0034] Then, the composite ceramic powder is added to distilled water, ball milled to form a slurry, coated on the surface ...
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