Method for preparing environment-friendly cigarette tows
A technology for tow and tobacco, which is applied in the field of preparation of environmentally friendly tobacco tow, can solve the problems of non-conformity with global sustainable development and domestic conditions, poor adhesion performance, insufficient drying, etc.
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Embodiment 1
[0043] Embodiment 1: Process investigation of polylactic acid
[0044] First of all, it needs to be explained that the raw material polylactic acid of the present invention can be commercially available, preferably polylactic acid (wherein the dextrorotatory D component weight percentage is 0-3%), or polylactic acid (wherein the dextrorotatory D component weight percent 0-3% content) and other materials blends or copolymers (wherein the proportion of polylactic acid is higher than 70%wt).
[0045] In order to better design the polylactic acid tow preparation process, the characteristics of polylactic acid have been deeply studied.
[0046] 1. The relationship between the physical properties of polylactic acid and the content of dextrorotatory D component
[0047] The synthetic raw material of polylactic acid, lactic acid or intermediate lactide, has stereoisomerism, so polylactic acid should be a homopolymer of the same optically active monomer or a copolymer of different opt...
Embodiment 2
[0058] Embodiment 2: the preparation method of modified polylactic acid tow
[0059] 1. The raw material chips are polylactic acid (component D content is 1%wt), intrinsic viscosity is 1.53dl / g, melt index is 23.5g / 10min (210°C, 2160g), glass transition temperature is 62°C, and melting temperature is 170°C.
[0060] 2. The preparation process of tow is:
[0061] 1) Carry out stepwise heating and drying crystallization in the range of 70-110°C (heating rate 5°C / h, the temperature remains unchanged when the temperature reaches 110°C), the time is 12 hours, and the water content in the polymer is 70ppm;
[0062] 2) Melt spinning, the number of holes in the spinneret is 12000, the spinneret holes are trilobal, the temperature of the spinning screw is controlled at 235±1°C, the temperature of the box is 230±1°C, and the spinning speed is 65m / min , the roller is oiled, the roller speed is 16m / min, the oil concentration is 1%; the cooling air adopts inner ring radiation cooling, the...
Embodiment 3
[0067] Embodiment 3: the preparation method of polylactic acid tow
[0068] 1. The raw material slices are commercially available polylactic acid from Natureworks Company, the brand name is 6400D.
[0069] 2. The preparation process of tow is:
[0070] 1) Carry out stepwise heating and drying crystallization in the range of 50-90°C (heating rate 5°C / h, the temperature remains unchanged when the temperature reaches 90°C), the time is 18 hours, and the water content in the polymer is 85ppm;
[0071] 2) Melt spinning, the number of holes in the spinneret is 12000, the spinneret holes are trilobal, the temperature of the spinning screw is controlled at 225±1°C, the temperature of the box is 220±1°C, and the spinning speed is 65m / min , the roller is oiled, the roller speed is 16m / min, the oil concentration is 1%; the cooling air adopts inner ring radiation cooling, the cooling temperature is 18±1℃, and the wind pressure is 700Pa;
[0072] 3) Five rolls with drafting preheating at...
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