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Method for preparing polishing solution by utilizing tailings recovered from crystal silicon cutting waste mortar

A technology for crystalline silicon cutting and waste mortar, applied in the direction of polishing compositions containing abrasives, etc., can solve the problems of crystalline silicon material loss, lack of recycling and comprehensive utilization technology, etc., achieve high-efficiency grinding ability, improve suspension, and polish smooth surface effect

Inactive Publication Date: 2013-09-18
JIANGSU JIAYU RESOURCE UTILIZATION
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] As we all know, more than 50% of the crystalline silicon in the silicon wafer production process is cut into silicon powder and enters the slurry. Due to the lack of effective recycling and comprehensive utilization technologies, such a large amount of crystalline silicon materials are lost in vain every year.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Take 100Kg of the tailings material in the recycling process of crystalline silicon cutting waste mortar, after testing, the silicon component (Si+SiO 2 ) content 20.6%, silicon carbide content 63.4%, cutting fluid component content 2.5%, metal component content 1.5%, moisture content 12%

[0020] Use a 12000 gauss magnetic bar to carry out magnetic separation on the above-mentioned tailing sand material, and detect that the metal component content of the sand material after magnetic separation is 0.42%; then add 350g of concentrated sulfuric acid to further remove the metal component in the sand material system, pickle, wash with water Finally, the metal component content in the sand was detected to be 0.07%. After precision filtration, 55.5Kg of concentrated slurry was obtained.

[0021] After adding 220kg of pure water to the concentrated slurry and stirring evenly, it enters the wet ultra-fine stirring mill in a fed-in manner, and at the same time feeds 170kg of 4....

Embodiment 2

[0025] Take 1000Kg of the tailings material in the recycling process of crystalline silicon cutting waste mortar resource recovery, wherein the silicon component in the solid (Si+SiO 2 ) content of 21.4%, silicon carbide content of 62.8%, PEG content of 2.4%, iron powder content of 1.4%, and moisture content of 12.2%.

[0026] Utilize the 12000 Gauss magnetic separator to carry out magnetic separation to the above-mentioned tailings sand material, detect the metal component content of the sand material after the magnetic separation is 0.32%; add 3Kg concentrated sulfuric acid to further remove the metal component in the sand material system, pickling 1. After washing with water, the metal component content in the sand material is detected to be 0.05%. After precision filtration, 557Kg of concentrated slurry was obtained.

[0027] After adding 2200kg of pure water to the concentrated slurry and stirring evenly, it enters the wet ultra-fine stirring mill in a fed-in manner, and...

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PUM

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Abstract

The invention discloses a method for preparing a polishing solution by utilizing tailings in the process of recycling crystal silicon cutting waste mortar. The method comprises the following steps of: deironing by two steps, grinding, converting, stabilizing and the like. According to the method, the problems that silicon powder is passivated, silicon carbide is wrapped by silica sol and the like are solved effectively by a crushing and grinding process of a wet-method superfine stirring mill, wherein the solation conversion rate of a silicon component is over 98.5 percent. According to the method, silicon carbide of less than 5 micrometers and the silicon component resources are utilized comprehensively, the prepared novel silicon carbide and silica sol composite polishing solution has the high-efficiency grinding capacity of the silicon carbide, and silicon dioxide sol can be embedded into gaps of a textured surface in a polishing surface, so that the polishing surface is smooth.

Description

technical field [0001] The invention relates to a method for preparing a polishing liquid by using the tailing material in the resource recycling process of crystal silicon cutting waste mortar. Its application field is mainly the environmental protection of the resource recycling industry of crystal silicon cutting waste mortar, and realizes the comprehensive utilization of silicon component resources and ultra-fine silicon carbide. Background technique [0002] Silicon wafers are an important foundation for the development of the solar industry. With the rapid development of the global solar energy industry, the demand and processing volume of silicon wafers are increasing. According to industry statistics, China's silicon wafer production capacity has ranked first in the world since 2008. In 2010, the total domestic silicon wafer production capacity was nearly 14GW, accounting for more than 50% of the global total production capacity. [0003] Wire cutting is currently ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09G1/02
Inventor 刘来宝冯国栋
Owner JIANGSU JIAYU RESOURCE UTILIZATION
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