Preparation method of heat conduction paster adopting fiber glass mesh as supporting structure
A technology of glass fiber mesh and support structure, which is applied in the direction of film/sheet adhesive, non-polymer adhesive additive, adhesive additive, etc. , increased fluidity, etc., to achieve the effects of excellent chemical stability, high thermal decomposition temperature, and improved coating performance
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Embodiment 1
[0019] (1) Dissolve 30g of silicone rubber in 90g of tetrahydrofuran to prepare a 25% silicone rubber solution, add 1.0g of double 2,5 silicone rubber vulcanizing agent, and stir evenly.
[0020] (2) Add 4 g of micron-sized aluminum oxide, 2 g of nano-AlN thermally conductive fillers, and 0.015 g of silane coupling agent KH-550 into step (1).
[0021] (3) In step (2), the mixed solution was ultrasonically dispersed for 20 minutes with a power of 800W.
[0022] (4) The mixed liquid in step (3) is put into a ball mill tank and ball milled for 24 hours to obtain a silicone rubber slurry in which the thermally conductive filler is uniformly dispersed.
[0023] (5) Soak the glass fiber mesh with concentrated sulfuric acid for 4 hours to obtain a pretreated glass fiber mesh.
[0024] (6) The slurry obtained in step (4) is uniformly coated on the pretreated glass fiber web in step (5).
[0025] (7) The silicon rubber-coated glass fibers obtained in step (6) were dried in a vacuum d...
Embodiment 2
[0028] (1) Dissolve 30g of silicone rubber in 70g of tetrahydrofuran to prepare a 30% silicone rubber solution, add 0.6g of double 2,5 silicone rubber vulcanizing agent, and stir evenly.
[0029] (2) Add 6 g of carbon-coated copper nanoparticle heat-conducting filler to step (1), and add 0.06 g of silane coupling agent Dow Corning Z-6020.
[0030] (3) In step (2), the mixed solution was ultrasonically dispersed for 30 minutes with a power of 1200W.
[0031] (4) The mixed solution in step (3) is put into a ball mill tank and ball milled for 2 hours to obtain a silicone rubber slurry in which the thermally conductive filler is uniformly dispersed.
[0032] (5) Soak the glass fiber mesh with concentrated sulfuric acid for 24 hours to obtain a pretreated glass fiber mesh.
[0033] (6) The slurry obtained in step (4) is uniformly coated on the pretreated glass fiber web in step (5).
[0034] (7) The silicon rubber-coated glass fibers obtained in step (6) were dried in a vacuum dr...
Embodiment 3
[0037] (1) Dissolve 30g of silicone rubber in 45g of tetrahydrofuran to prepare a 40% silicone rubber solution, add 0.45g of double 2,5 silicone rubber vulcanizing agent, and stir evenly.
[0038] (2) Add 9g of nanometer AlN particle thermal conductive filler to step (1), and add 0.045g of silane coupling agent Dow Corning Z-6040.
[0039] (3) In step (2), the mixed liquid was ultrasonically dispersed for 40 minutes, and the power was 1200W.
[0040] (4) The mixed liquid in step (3) is put into a ball mill tank and ball milled for 24 hours to obtain a silicone rubber slurry in which the thermally conductive filler is uniformly dispersed.
[0041] (5) Soak the glass fiber mesh with a mixed strong acid of concentrated sulfuric acid and concentrated nitric acid for 20 hours to obtain a pretreated glass fiber mesh.
[0042] (6) The slurry obtained in step (4) is uniformly coated on the pretreated glass fiber web in step (5).
[0043] (7) The glass fiber coated with silicone rubber...
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