Organosilicon waterproofing agent and preparation method thereof
A technology of silicone and water repellent, applied in the direction of coating, etc., can solve the problems of coating swelling, coating life reduction, cracking, etc., and achieve the effect of low production cost, convenient operation and low pollution
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[0017] A kind of preparation method of organosilicon waterproofing agent, it is characterized in that: it comprises the following steps:
[0018] The first step is to add a strong base into the hydrogen-containing silicone oil and stir to obtain a silicone resin; wherein the mass ratio of the hydrogen-containing silicone oil to the strong base is 100:1-10.
[0019] The second step is to dissolve the above-mentioned silicone resin with an organic solvent, then add a small amount of tetramethylammonium hydroxide as a catalyst, stir and heat up to the boiling point to make it crack; wherein the silicone resin and organic solvent and tetramethylammonium The mass ratio of ammonium hydroxide is: 1:10-20:0.01.
[0020] In the third step, the above product is cooled to room temperature, diluted with water, and the product is separated.
Embodiment 1
[0022] Prepare the silicone waterproofing agent according to the above steps, wherein the hydrogen-containing silicone oil is 100 g, the strong base is 1 g, the organic solvent is 1000 g, and the tetramethylammonium hydroxide is 1 g.
Embodiment 2
[0024] Prepare the silicone waterproofing agent according to the above steps, wherein the hydrogen-containing silicone oil is 100g, the strong base is 5g, the organic solvent is 1000g, and tetramethylammonium hydroxide is 1g.
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