Method for preparing metal titanium or titanium alloy super-oleophobic surface
A technology of titanium alloy and metal titanium is applied in the field of preparation of superoleophobic surface of metal titanium or titanium alloy, which can solve problems such as the difficulty of superoleophobic surface, achieve simple and mature preparation process, improve conveying speed, and reduce water resistance. Effect
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Embodiment 1
[0022] 1. With the cleaned metal titanium as the anode and the graphite sheet as the cathode, the metal titanium is mixed with 0.1wt% Na 2 SO 4 Carry out anodic oxidation once in aqueous solution, the oxidation current is 0.1A / cm 2 , the oxidation time is 2h, and after the reaction is completed, the oxide and floating liquid are removed by ultrasonic cleaning, and a titanium-based surface with a micron structure is roughened;
[0023] 2. Use micron-structured roughened titanium as the anode, graphite sheet as the cathode, and 0.1wt% HCl aqueous solution as the electrolyte for secondary anodic oxidation. The oxidation voltage is 10V, the oxidation time is 2 hours, and the temperature is 0-5 ℃, forming a uniform layer of titanium oxide nanotube arrays on the micronized titanium surface to obtain a micro-nano structured titanium surface;
[0024] 3. Spin-coat perfluorooctadecyltrichlorosilane on the micro-nano structured titanium surface for chemical modification, and heat trea...
Embodiment 2
[0027] 1. With the cleaned metal titanium as the anode and the graphite sheet as the cathode, the metal titanium is anodized once in 5wt% NaOH aqueous solution, and the oxidation current is 0.5A / cm 2 , the oxidation time is 1h, and after the reaction is completed, the oxide and floating liquid are removed by ultrasonic cleaning, and a titanium-based surface with a micron structure is roughened;
[0028] 2. Use micron-structured roughened titanium as the anode, graphite sheet as the cathode, and 5wt% HCl ethylene glycol solution as the electrolyte for secondary anodic oxidation. The oxidation voltage is 100V, the oxidation time is 10min, and the temperature is 10°C , forming a layer of uniform titanium oxide nanotube arrays on the micronized titanium surface to obtain a micro-nano structured titanium surface;
[0029] 3. Spin-coat perfluorooctadecyltrichlorosilane onto the dried micro-nano structured titanium surface for chemical modification, and heat-treat at 100°C for 1 hour...
Embodiment 3
[0032] 1. With the cleaned titanium alloy as the anode and the graphite sheet as the cathode, the metal titanium is mixed with 5wt% Na 2 SO 4 Carry out anodic oxidation once in ethylene glycol solution, the oxidation current is 1A / cm 2 , the oxidation time is 0.5h, and after the reaction is completed, the oxide and floating liquid are removed by ultrasonic cleaning, and a titanium-based surface with a micron structure is roughened;
[0033] 2. Use titanium with a rough surface microstructure as the anode, graphite sheet as the cathode, and 0.1wt% HF formamide solution as the electrolyte for secondary anodic oxidation. The oxidation voltage is 20V, the oxidation time is 30min, and the temperature is 0 ℃, forming a uniform layer of titanium oxide nanotube arrays on the micronized titanium surface to obtain a micro-nano structured titanium surface;
[0034] 3. Deposit perfluorooctyl siloxane on the dry micronano-structured titanium surface by vapor deposition method for chemica...
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