Fluorescent powder coating liquid of white light emitting diode as well as preparation method and coating method thereof
A technology of light-emitting diodes and phosphors, applied in luminescent coatings, devices for coating liquid on the surface, coatings, etc., can solve the problem of further migration, sedimentation or agglomeration of phosphors, inability to effectively protect against ultraviolet radiation, and LED color drift etc. to improve reliability and stability, reduce attenuation, and reduce thermal quenching
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Embodiment 1
[0025] Embodiment 1: Phosphor powder coating solution is composed of silica sol, phosphor powder and deionized water with weight percentages of 60%, 35% and 5%, respectively. Among them, the silica sol is an inorganic compound nano-silica sol; the function of deionized water is to adjust the viscosity of the coating solution. In other embodiments, distilled water can be used instead of deionized water; in further embodiments, reinforcing agents, plasticizers and dispersants can also be added as additives.
[0026] The silica sol in this embodiment belongs to the nano glue, and the nano glue itself has a "coating" effect on the phosphor powder, which reduces the damage of ultraviolet radiation to the phosphor powder and reduces the thermal quenching of the phosphor powder, thereby reducing the phosphor powder. Attenuation and color drift of light-emitting diodes and improve the aging resistance of light-emitting diodes. The phosphor powder coating liquid of the white light emi...
Embodiment 2
[0028] Example 2: At room temperature, slowly pour 60% of neutral silica sol, 5% of deionized water, and other additives (such as reinforcing agent, plasticizer, and dispersant) into a ball mill filled with 35% phosphor In the tank, add a certain amount of grinding balls to mix the mill. Wherein the weight ratio of the agate grinding balls whose diameters are respectively φ6, φ10, φ15 depends on the required particle size, and the preferred ratio of this example is 2:1:1. The speed of the ball mill is 90n / min, and the grinding time is about 4 hours. The silica sol in this embodiment is an inorganic polymer after being cured, which does not generate segmental thermal movement, and has better compatibility with the inorganic phosphor. The reliability and stability of the LED are thus improved.
[0029] An embodiment of the present invention provides a coating method based on the above-mentioned phosphor coating liquid for white light emitting diodes. The coating liquid is adde...
Embodiment 3
[0030]Embodiment 3: Add the prepared coating solution to the liquid precision quantitative dispensing device to dispensing and coating the LED chip, and place the coated chip in an oven at 100-150°C for 20-30 minutes to let the solvent evaporate completely , and then resin encapsulation process. Among them, an oven curing condition of 120° C. and 20-30 minutes is the preferred solution. Compared with traditional organic packaging materials, the above coating liquid has a higher refractive index, which can further improve the light extraction efficiency of packaging devices.
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