Phase-change heat conductive material and preparation method thereof
A phase-change heat-conducting and heat-conducting powder technology, applied in heat exchange materials, chemical instruments and methods, etc., can solve the problems of increasing thermal resistance, drying out, loss, etc., to achieve accelerated heat transfer, convenient disassembly and assembly, high thermal conductivity sexual effect
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Embodiment 1
[0040] (1) Put 20g of EPDM, 10g of paraffin wax, 18.5g of polyborosiloxane tackifier, and 10g of silicone resin with a viscosity of 60cps into the heating and stirring tank to stir and mix them evenly at a temperature of 150°C.
[0041] (2) Take by weighing 40g of aluminum oxide with an average particle diameter of 40 microns after impregnating and drying the ethanol solution containing 1.5g of n-hexyltrimethoxysilane, put into the stirring tank in step (1) and vacuumize and stir for 1 hours to make the raw material mixture.
[0042] (3) The raw material mixture is roll-coated on a 0.025mm thick Kapton MT film at 80°C, and it becomes a phase-change thermally conductive material after cooling.
[0043] (4) Put the phase-change heat-conducting material in step (3) into the device for testing the hardness for testing.
[0044] (5) Put the phase-change thermally conductive material in step (3) into a device for detecting thermal conductivity to detect thermal conductivity.
[00...
Embodiment 2
[0047] (1) Put 2g of EPDM, 18g of paraffin wax, 5g of polyborosiloxane tackifier, and 10g of silicone resin with a viscosity of 3000cps into a heating and stirring tank to stir and mix them evenly at a temperature of 150°C.
[0048] (2) Weighing 64g of aluminum nitride with an average particle diameter of 40 microns and magnesium oxide with an average particle diameter of 60 microns, impregnated with an ethanol solution containing 1g of n-decyltriethoxysilane, dried, and put into Vacuumize and stir in the stirring tank of step (1) for 1 hour to make a raw material mixture.
[0049] (3) Roll coat the raw material mixture on a 0.013mm thick PEN film at 80°C, and form a phase-change thermally conductive material after cooling.
[0050] (4) Put the phase-change heat-conducting material in step (3) into the device for testing the hardness for testing.
[0051](5) Put the phase-change thermally conductive material in step (3) into a device for detecting thermal conductivity to dete...
Embodiment 3
[0054] (1) Put 10g of EPDM, 5g of paraffin wax, 5g of polyborosiloxane tackifier, and 39g of silicone resin with a viscosity of 5000cps into the heating and stirring tank to stir and mix them evenly at a temperature of 150°C.
[0055] (2) taking by weighing 40g average particle diameter is the boron nitride of 80 microns through the ethanol solution impregnation treatment containing n-octyltriethoxysilane 1g, after drying, put into the stirring tank of step (1) and vacuum stir for 1 hours to make the raw material mixture.
[0056] (3) After the raw material mixture is pressed into tablets and cooled, it becomes a phase-change heat-conducting material.
[0057] (4) Put the phase-change heat-conducting material in step (3) into the device for testing the hardness for testing.
[0058] (5) Put the phase-change thermally conductive material in step (3) into a device for detecting thermal conductivity to detect thermal conductivity.
[0059] The test data shows that the thickness...
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