Process for preparing permanent magnet iron oxygen body polymer composite magnet
A technology of permanent ferrite and composite magnets, applied in the direction of magnetism of organic materials/organic magnetic materials, can solve the problems of complex process, low mixing efficiency, high mixing equipment and process requirements, simplify the preparation process, overcome the mixing The effect of high equipment and process requirements
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Embodiment 1
[0023] In terms of parts by mass, 3 parts of KH550 and 100 parts of strontium ferrite magnetic powder are mixed uniformly, then fully dried, and the surface of the magnetic powder is coated. Subsequently, in parts by mass, 6 parts of dibenzoyl peroxide are added to 100 parts of methyl methacrylate monomer to make methyl methacrylate monomer solution; 10 parts of monomer solution are mixed with the above Mix 90 parts of strontium ferrite magnetic powder after one-step treatment to prepare a suspension system, then heat the suspension system to 90°C in nitrogen and keep it warm for 8 hours to make the methyl methacrylate monomer undergo in-situ polymerization on the surface of the magnetic powder Polymethyl methacrylate is produced. Finally, using a twin-screw extruder at 190°C, the magnetic powder coated with polymethyl methacrylate was directly extruded under the action of a 1000kA / m orientation magnetic field to prepare the strontium ferrite powder—polymethyl methacrylate Es...
Embodiment 2
[0025] In terms of parts by mass, mix 6 parts of KH550 and 100 parts of strontium ferrite magnetic powder evenly, then fully dry, and carry out surface coating treatment on the magnetic powder; Add 7 parts of azobisisobutyronitrile in the glyceride monomer to make methyl methacrylate glycidyl ester monomer melt; and 10 parts of monomer solution with 90 parts of strontium iron Mix oxygen and magnetic powder to prepare a suspension system; heat the suspension system to 70°C in nitrogen and keep it warm for 7 hours, so that methyl methacrylate glycidyl ester monomer can undergo in-situ polymerization reaction on the surface of the magnetic powder to form polymethyl methacrylate Ester glycidyl ester. Finally, using a single-screw extruder at 130°C, the magnetic powder coated with polymethyl methacrylate glycidyl ester was directly extruded under the action of a 1000kA / m orientation magnetic field to prepare the strontium ferrite powder—polymethylmethacrylate. Glycidyl methyl acry...
Embodiment 3
[0027]In terms of parts by mass, 5 parts of KH550 and 100 parts of strontium ferrite magnetic powder are mixed uniformly, then fully dried, and the surface of the magnetic powder is coated. Subsequently, in terms of parts by mass, 6 parts of azobisisobutyronitrile were added to 100 parts of butyl acrylate to make a butyl acrylate melt; 10 parts of the solution were mixed with 90 parts of strontium iron oxide The suspension system was prepared by mixing the magnetic powder with the magnetic powder; the suspension system was heated to 65° C. in nitrogen and kept for 5 hours, so that the butyl acrylate monomer was in-situ polymerized on the surface of the magnetic powder to form polybutyl acrylate. Finally, using a twin-screw extruder at 120°C, the polybutylacrylate-coated magnetic powder formed by polymerization is directly extruded under the action of a 1000kA / m orientation magnetic field to prepare the strontium ferrite powder-polybutylacrylate composite magnet. After testing...
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