High-strength and deformation-resistant TPO waterproof coiled material and preparation method thereof
A waterproof membrane and anti-deformation technology, applied in chemical instruments and methods, rubber layered products, layered products, etc., can solve problems such as large stress relaxation rate, large stress drop, and performance damage, and achieve a stress relaxation rate Small size, good low-temperature bendability, and good tensile properties
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Embodiment 1
[0041] (1) Preparation of modified ethylene-1-hexene copolymer
[0042] Mix nano-chromium boride and mullite, add tetrapropoxysilane and grind to a particle size of 2 μm to obtain modified mullite, mix modified mullite with ethylene-1-hexene copolymer and heat to copolymerize The product is melted, kept in a molten state and kneaded in a kneader, and extruded by a screw to obtain a modified ethylene-1-hexene copolymer;
[0043] The nano-chromium boride particle size is 80nm;
[0044] The alumina content in the mullite is 76%;
[0045] The weight average molecular weight of the ethylene-1-hexene copolymer is 150000-170000g / mol;
[0046] Described nano chromium boride and mullite mass ratio are 2:5;
[0047] Described tetrapropoxysilane and mullite mass ratio are 1:200;
[0048] The mass ratio of the modified mullite to the ethylene-1-hexene copolymer is 1:10.
[0049] (2) Preparation of reinforcement layer
[0050] The reinforcing layer includes the following components i...
Embodiment 2
[0073] (1) Preparation of modified ethylene-1-hexene copolymer
[0074] Mix nano-chromium boride and mullite, add tetrapropoxysilane and grind to a particle size of 1.5 μm to obtain modified mullite, mix modified mullite with ethylene-1-hexene copolymer and heat to The copolymer is melted, kept in a molten state and kneaded in a kneader, and extruded by a screw to obtain a modified ethylene-1-hexene copolymer;
[0075] The nano-chromium boride particle size is 70nm;
[0076] The alumina content in the mullite is 75%;
[0077] The weight average molecular weight of the ethylene-1-hexene copolymer is 140000-160000g / mol;
[0078] Described nano chromium boride and mullite mass ratio are 1.5:5;
[0079] Described tetrapropoxysilane and mullite mass ratio are 1:180;
[0080] The mass ratio of the modified mullite to the ethylene-1-hexene copolymer is 1:8.
[0081] (2) Preparation of reinforcement layer
[0082] The reinforcing layer includes the following components in parts ...
Embodiment 3
[0105] (1) Preparation of modified ethylene-1-hexene copolymer
[0106] Mix nano-chromium boride and mullite, add tetrapropoxysilane and grind to a particle size of 2.5 μm to obtain modified mullite, mix modified mullite with ethylene-1-hexene copolymer and heat to The copolymer is melted, kept in a molten state and kneaded in a kneader, and extruded by a screw to obtain a modified ethylene-1-hexene copolymer;
[0107] The nano-chromium boride particle size is 90nm;
[0108] The alumina content in the mullite is 77%;
[0109] The weight average molecular weight of the ethylene-1-hexene copolymer is 160000-180000g / mol;
[0110] Described nano-chromium boride and mullite mass ratio are 2.5:5;
[0111] Described tetrapropoxysilane and mullite mass ratio are 1:220;
[0112] The mass ratio of the modified mullite to the ethylene-1-hexene copolymer is 1:12.
[0113] (2) Preparation of reinforcement layer
[0114] The reinforcing layer includes the following components in parts...
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