A kind of preparation method of titanium alloy sheet
A technology for titanium alloys and plates, applied in the field of preparation of titanium alloy plates, can solve the problems of not yet realized industrial production application, unclear process parameters of ingot pretreatment, shaping and rolling, etc., achieving small grain size, reducing steps, reducing cost effect
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Embodiment 1
[0037] Example 1: Preparation of titanium alloy sheet (1)
[0038] (1) Using grade 0 sponge titanium and high-quality master alloys of aluminum and vanadium, the alloy ratio is carried out according to TC4 (Ti-6Al-4V). Welded into electrodes. The consumable vacuum arc furnace (VAR furnace) is used for three smelting, and the obtained ingot is turned and peeled by a lathe, and the riser is sawed to obtain a finished alloy ingot.
[0039](2) The ingot is heated to 850°C in a box-type resistance heating furnace, and kept for 100 minutes; then the temperature is increased to 1150°C, and the temperature is kept for 500 minutes. The heated ingot is shaped on a 4500T press, and the cylindrical ingot is pressed into a rectangular billet with a thickness of 300mm. After air cooling, use a grinding and polishing machine to polish off the oxide skin and debris on the surface of the blank, plan and mill on six sides on a gantry milling machine, smooth the surface, and mill out the uneve...
Embodiment 2
[0042] Example 2: Preparation of Titanium Alloy Plate (2)
[0043] (1) Using grade 0 sponge titanium and high-quality master alloys of aluminum, iron, chromium, tin and silicon, according to TC611 (Ti-(4-7)Al-(0.2-2.5)Fe-(0.1-2)Cr-(0.1 -2) Alloy ratio of Sn-(0.1-0.5)Si), the alloy with good ratio is pressed into alloy blocks on a 3000-ton hydraulic press, and welded into electrodes in a vacuum welding box. The consumable vacuum arc furnace (VAR furnace) is used for three smelting, and the obtained ingot is turned and peeled by a lathe, and the riser is sawed to obtain a finished alloy ingot.
[0044] (2) The ingot is heated to 800°C in a box-type resistance heating furnace, and kept for 100 minutes; then the temperature is increased to 1000°C, and the temperature is kept for 500 minutes. The heated ingot is shaped on a 4500T press, and the round ingot is pressed into a rectangular billet with a thickness of 200mm. After air cooling, use a grinding and polishing machine to po...
Embodiment 3
[0047] Example 3: Detection of titanium alloy sheets prepared in Example 1 and Example 2
[0048] The microstructures and morphologies of the titanium alloy sheets prepared in Examples 1 and 2 are as follows: figure 1 , 2 shown. from figure 1 and figure 2 It can be seen that the distribution of each phase inside the finished plate is uniform, and an ideal and fine equiaxed structure is obtained; after annealing, the plate is completely recrystallized, and the grain distribution is uniform, which meets the supply demand of titanium alloy plate.
[0049] Table 1 is based on the traditional process (ingot smelting-heating-forging upsetting-returning upsetting-air cooling grinding-heating upsetting-repair-heating forging-planing-milling-heating-rolling-heat treatment-acid-base washing-cutting planing Milling-finished product) prepared TC4 and TC611 titanium alloy plates (wherein ingot smelting, acid-base washing and subsequent procedures are consistent with the present invent...
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