Monocrystalline silicon texturing additive with strong dirt-removing power and application thereof
A technology of decontamination ability and crystalline silicon texturing, which is applied in the direction of single crystal growth, single crystal growth, sustainable manufacturing/processing, etc., and can solve problems such as increased alkali consumption, excessive adsorption, and slow texturing reaction
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Embodiment 1
[0033] This embodiment provides a method for making texturing of a monocrystalline silicon wafer, comprising the following specific steps:
[0034] (1) Preparation of the first surfactant: In terms of parts by mass, weigh 4.5 parts of decyldimethylallyl ammonium chloride as the hydrophobic monomer, 3 parts of allyl polyoxyethylene ether 800 and 22.5 parts of methyl Acrylic acid is used as a hydrophilic monomer, mixed with the rest of deionized water to prepare an aqueous solution with a concentration of 30% by mass; then sodium hydroxide is added to adjust the pH value of the aqueous solution to 6~8; Five parts of potassium persulfate is used as an oxidizing agent, and five parts per ten thousand of sodium sulfite is used as a reducing agent. The above substances are stirred evenly and copolymerized for 3 hours to obtain the first surfactant.
[0035] Preparation of additives for texturing: according to the parts by mass, weigh 15 parts of the above reaction product (including...
Embodiment 2
[0040] This embodiment provides a method for making texturing of a monocrystalline silicon wafer, comprising the following specific steps:
[0041] (1) Preparation of the first surfactant: according to the mass parts, weigh 3 parts of dodecyl dimethyl allyl ammonium chloride as the hydrophobic monomer, 3 parts of allyl polyoxyethylene ether 1000 and 24 parts Acrylic acid is used as a hydrophilic monomer, mixed with the remaining amount of deionized water to prepare an aqueous solution with a mass percentage concentration of 25%; then adding sodium hydroxide to adjust the pH value of the aqueous solution to 6~8; then adding the above-mentioned monomer mass 5 / 10,000 parts of potassium persulfate was used as an oxidizing agent, and 5 / 10,000 parts of sodium sulfite was used as a reducing agent. The above substances were stirred evenly and copolymerized for 3 hours to obtain the first surfactant.
[0042] Preparation of additives for texturing: according to the parts by mass, weig...
Embodiment 3
[0047] (1) Preparation of the first surfactant: according to the mass parts, weigh 3 parts of hexadecyl dimethyl allyl ammonium chloride as the hydrophobic monomer, 3 parts of allyl polyoxyethylene ether 1200 and 24 parts Acrylic acid is used as a hydrophilic monomer, mixed with the remaining amount of deionized water to prepare an aqueous solution with a concentration of 20% by mass; then sodium hydroxide is added to adjust the pH value of the aqueous solution to 6~8; 10000 parts of potassium persulfate was used as an oxidizing agent, and 8 / 10000 parts of sodium sulfite was used as a reducing agent. The above substances were stirred evenly and copolymerized for 3 hours to obtain the first surfactant.
[0048] Preparation of texturing additives: according to the mass parts, weigh 12 parts of the above reaction product (containing 3.6 parts of active ingredients) as the first surfactant, 0.2 parts of oleic acid diethanolamide and 2 parts of sodium dodecylbenzenesulfonate As the...
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