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Dyeing auxiliary and application thereof to dyeing assistance of disperse dyes

A technology of dyeing auxiliaries and mass fraction, applied in dyeing method, textile and papermaking, etc., can solve the problems of complex extraction and processing, high cost, and achieve obvious solubilization and dyeing effect, low cost, and increase the percentage of dyeing.

Inactive Publication Date: 2019-01-18
卢梅雅
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, as a natural surfactant, lipids are more complicated to extract and process, and the cost is also higher.

Method used

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  • Dyeing auxiliary and application thereof to dyeing assistance of disperse dyes
  • Dyeing auxiliary and application thereof to dyeing assistance of disperse dyes
  • Dyeing auxiliary and application thereof to dyeing assistance of disperse dyes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The present embodiment is a kind of dyeing auxiliaries, in terms of mass fraction, the dyeing auxiliaries include the following components: Pingpingjia O-1540%, PEG-23 stearate 4%, triethylene glycol monobutyl ether 5%, Octadecyl Betaine 3%, Lauryl Dihydroxyethyl Betaine 5%, Polyamide Polyamine Epichlorohydrin 10%, Chitosan 3%;

[0032] Wherein, the average molecular weight of polyamide polyamine epichlorohydrin is 8000D;

[0033] The degree of deacetylation of chitosan is 75%, and the average molecular weight is 4000D.

[0034] Wool is dyed with the above dyeing auxiliaries and Disperse Red M-BL, including:

[0035] (1) Make wool into rolls, soak in 2g / L hexamethylenediamine liquid for 20min, wash with deionized water, and set aside;

[0036] (2) Mix the dyeing auxiliaries and disperse dyes at a mass ratio of 1:3, add water to 1000mL, make the concentration of the dyeing auxiliaries in the dye bath 4g / L, and use glacial acetic acid to adjust the pH of the dye bath to...

Embodiment 2

[0041] The present embodiment is a kind of dyeing auxiliaries, in terms of mass fraction, the dyeing auxiliaries include the following components: Pingpingjia O-30 68%, PEG-18 stearate 3%, triethylene glycol monobutyl ether 8%, Octadecyl Betaine 5%, Lauryl Dihydroxyethyl Betaine 4%, Polyamide Polyamine Epichlorohydrin 8%, Chitosan 4%;

[0042] Wherein, the average molecular weight of polyamide polyamine epichlorohydrin is 12000D;

[0043] The degree of deacetylation of chitosan is 85%, and the average molecular weight is 5000D.

[0044] Wool is dyed with the above dyeing auxiliaries and Disperse Red M-BL, including:

[0045] (1) Make wool into rolls, soak in 2g / L hexamethylenediamine liquid for 20min, wash with deionized water, and set aside;

[0046] (2) Mix the dyeing auxiliaries and disperse dyes at a mass ratio of 1:3, add water to 1000mL, make the concentration of the dyeing auxiliaries in the dye bath 6g / L, and use glacial acetic acid to adjust the pH of the dye bath to ...

Embodiment 3

[0051] The present embodiment is a kind of dyeing auxiliaries, in terms of mass fraction, the dyeing auxiliaries include the following components: Pingpingjia O-20 56%, polyoxyethylene-20 stearate 4%, triethylene glycol monobutyl ether 6 %, octadecyl betaine 7%, dodecyl dihydroxyethyl betaine 2%, polyamide polyamine epichlorohydrin 6%, chitosan 5%;

[0052] Wherein, the average molecular weight of polyamide polyamine epichlorohydrin is 10000D;

[0053] The degree of deacetylation of chitosan is 80%, and the average molecular weight is 4500D.

[0054] Wool is dyed with the above dyeing auxiliaries and Disperse Red M-BL, including:

[0055] (1) Make wool into rolls, soak in 2g / L hexamethylenediamine liquid for 20min, wash with deionized water, and set aside;

[0056] (2) Mix the dyeing auxiliaries and disperse dyes at a mass ratio of 1:3, add water to 1000mL, make the concentration of the dyeing auxiliaries in the dye bath 5g / L, and use glacial acetic acid to adjust the pH of ...

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Abstract

The invention discloses a dyeing auxiliary and an application thereof to dyeing assistance of disperse dyes. The dyeing auxiliary comprises following components in percentage by mass: 40%-68% of polyoxyethylene aliphatic alcohol ether, 2%-4% of polyoxyethylene stearate, 5%-8% of triethylene glycol monobutyl ether, 5%-12% of N-alkyl betaine, 6%-10% of polyamide-polyamine-epichlorohydrin and 3%-5% of chitosan. According to the dyeing auxiliary, polyoxyethylene aliphatic alcohol ether is taken as a main component, polyoxyethylene stearate is added to realize compounding synergistic interaction with polyoxyethylene aliphatic alcohol ether, and therefore, the solubilizing dyeing effect of the dyeing auxiliary is improved; the dyes are promoted to be more powerfully combined with fibers with addition of triethylene glycol monobutyl ether, cloud point of polyoxyethylene aliphatic alcohol ether is increased with addition of N-alkyl betaine, contact probability of the dyes and the fibers is increased with addition of polyamide-polyamine-epichlorohydrin, diffusion rate of the dyes in the fibers is increased with addition of chitosan, and dye uptake of the dyes is increased.

Description

technical field [0001] The invention relates to the technical field of disperse dye dyeing, in particular to a dyeing auxiliary and its application in assisting disperse dyes in dyeing. Background technique [0002] As we all know, the dyeing speed of dyes to fibers is not only determined by the molecular structure of dyes and fibers, but also related to the solubility of dyes in the dye bath and the degree of swelling or plasticization of fibers during dyeing. And choose appropriate auxiliaries, increase the solubility of insoluble dyes in the dye bath, can speed up the adsorption of dyes to fibers, if the auxiliaries can solubilize or plasticize fibers, it can also accelerate the diffusion of dyes in fibers speed, which can speed up the entire dyeing speed. [0003] The effect of solubilizing dyeing with additives is mainly reflected in the following four aspects: (1) increase the solubility of insoluble dyes; (2) accelerate the adsorption of dyes to the surface of fibers...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/613D06P1/651D06P1/66D06P1/52D06P1/46D06P1/16D06P3/14
CPCD06P1/16D06P1/46D06P1/5264D06P1/6133D06P1/6136D06P1/65131D06P1/66D06P3/143D06P5/002
Inventor 卢梅雅
Owner 卢梅雅
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