Preparation method of monolithic interlayer through hole
A single-layer, silicon wafer technology, applied in chemical instruments and methods, semiconductor/solid-state device manufacturing, electrical components, etc., can solve the problems of residual contamination of reactive gases, different etching rates, non-uniformity, etc., and achieve good through holes. Etching quality, the effect of eliminating the inclination problem
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preparation example 1
[0063] This preparation example provides a kind of etching solution containing bacillus licheniformis, described etching solution containing bacillus licheniformis is prepared by following preparation method:
[0064] (a) Inoculate Bacillus licheniformis into NA medium and culture at 37°C for 24h, centrifuge at 2000rpm for 10min to remove the secretion of Bacillus licheniformis, aggregate and purify to obtain Bacillus licheniformis;
[0065] (b) Get 300mL of Bacillus licheniformis obtained by aggregation and purification, add 700mL of phosphate buffer solution with a pH value of 7.4, and then cultivate for 4 hours in an environment with a temperature of 37°C to obtain 300,000 live bacteria containing Bacillus licheniformis etchant.
preparation example 2
[0067] This preparation example provides a kind of etching solution containing Bacillus cereus, and the etching solution containing Bacillus cereus is prepared by the following preparation method:
[0068] (a) Inoculate Bacillus cereus into Chua's medium and culture at 37°C for 24 hours, centrifuge at 1800 rpm for 8 minutes to remove the secretion of Bacillus cereus, aggregate and purify to obtain Bacillus cereus;
[0069] (b) Take 300mL of aggregated and purified Bacillus cereus and add 700mL of phosphate buffer solution with a pH value of 7.4, and then culture in an environment with a temperature of 37°C for another 6 hours to obtain a viable count of 320,000 cereus-containing spores Bacillus etchant.
preparation example 3
[0071] This preparation example provides a kind of etching solution containing Alcaligenes faecalis, and the etching solution containing Alcaligenes faecalis is prepared by the following preparation method:
[0072] (a) inoculate Alcaligenes faecalis in Chua's medium and cultivate at 30°C for 24h, remove the excretion of Alcaligenes faecalis by centrifuging at 1500rpm for 10min, gather and purify to obtain Alcaligenes faecalis;
[0073] (b) Add 300mL of Alcaligenes faecalis obtained by aggregation and purification into 700mL of phosphate buffer with a pH value of 7.4, and then culture for another 5 hours in an environment with a temperature of 30°C to obtain 350,000 viable bacteria containing Alcaligenes faecalis bacteria etchant.
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