Amino acid shampoo with oil control and dandruff removal effects and preparation method thereof
An amino acid and shampoo technology, applied in medical preparations containing active ingredients, chemical instruments and methods, hair care, etc., to achieve excellent oil control and dandruff removal, improve compatibility, and reduce agglomeration effects.
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Embodiment 1
[0034] Embodiment 1, oil control anti-dandruff composition
[0035] Nanoporous silica preparation:
[0036] S1, add water 10m to the reactor 3 and sodium silicate solution 3m 3 , heated to 75°C, while stirring, add sulfuric acid solution dropwise at an even speed until the pH is 9.0, stop dropping, and stir for 8 minutes;
[0037] S2. Heat to 85°C, add 2.5m sodium silicate solution while stirring 3 , continue heating to 95°C, add sulfuric acid solution at an even rate until the pH is 3.5, stop the dropwise addition, and stir for 5 minutes to obtain a silica slurry;
[0038] S3. Press filter the above silica slurry, wash, spray dry, pulverize, add 30% ethanol solution to obtain a mixed solution; freeze the mixed solution at -20°C, take it out at room temperature after complete freezing Thaw until it is completely thawed, so freeze and thaw cycles 12 times, filter, collect the filter cake, wash with deionized water, spray dry, pulverize, porous silica.
[0039] Wherein, the ...
Embodiment 2
[0046] Embodiment 2, oil control anti-dandruff composition
[0047] Nanoporous silica preparation:
[0048] S1, add water 12m into the reactor 3 and sodium silicate solution 3m 3 , heated to 75°C, while stirring, add sulfuric acid solution dropwise at an even speed until the pH is 8.5, stop dropping, and stir for 8 minutes;
[0049] S2. Heat to 85°C, add 2.5m sodium silicate solution while stirring 3 , continue heating to 90°C, add sulfuric acid solution at an even rate until the pH is 3.0, stop the dropwise addition, and stir for 8 minutes to obtain a silica slurry;
[0050] S3. Press filter the above silica slurry, wash, spray dry, and pulverize, add 50% ethanol solution to obtain a mixed solution; freeze the mixed solution at -20°C, and take it out at room temperature after being completely frozen. Thaw until it is completely thawed, so freeze and thaw cycle 15 times, filter, collect the filter cake, wash with deionized water, spray dry, pulverize, porous silica.
[...
Embodiment 3
[0058] Embodiment 3, oil control anti-dandruff composition
[0059] Nanoporous silica preparation:
[0060] S1, add 8m of water to the reactor 3 and sodium silicate solution 2.5m 3 , heated to 70°C, while stirring, add sulfuric acid solution dropwise at an even speed until the pH is 9.5, stop dropping, and stir for 8 minutes;
[0061] S2. Heat to 85°C, add 1.5m sodium silicate solution while stirring 3 , continue heating to 90°C, add sulfuric acid solution at an even rate until the pH is 3.5, stop the dropwise addition, and stir for 8 minutes to obtain a silica slurry;
[0062] S3. Press filter the above silica slurry, wash, spray dry, pulverize, add 60% ethanol solution to obtain a mixed solution; freeze the mixed solution at -20°C, and take it out at room temperature after it is completely frozen. Thaw until it is completely thawed, so freeze and thaw cycles 10 times, filter, collect the filter cake, wash with deionized water, spray dry, pulverize, porous silica.
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