Preparation method of mesoporous MSQ aerogel/glass fiber composite material
A technology of glass fiber and composite materials, applied in the field of thermal insulation materials, to achieve the effect of improving mechanical properties and improving thermal insulation performance
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Embodiment 1
[0030] Embodiment 1: see figure 1
[0031] A preparation method of a mesoporous MSQ airgel / glass fiber composite material containing an infrared shading agent, comprising the following steps:
[0032] 1) Mix and stir 32 g of cetyltrimethylammonium chloride, 100 mL of methyltrimethoxysilane, 250 mL of methanol and 50 mL of hydrochloric acid (0.001 mol / L), then add 250 mL of 1 -2 propylene oxide, stirred for 2 min and then poured into a fixed container to obtain a sol; add 25mL of titanium sol to the sol and fully stir to obtain a composite sol;
[0033] 2) Completely impregnate the cut high-silica glass fiber mat in the composite sol, transfer the glass fiber mat impregnated with the composite sol into a plastic box and seal it;
[0034] 3) Put the sealed plastic box in a microwave dryer for microwave curing, set the dehumidification rate to 20%, microwave power to 250 W, and curing time to 12 minutes; add methanol to the obtained gel / glass fiber composite material for solven...
Embodiment 2
[0037] Embodiment 2: see figure 2
[0038] A preparation method of mesoporous MSQ airgel / glass fiber composite material containing an infrared opacifying agent, the volume of the titanium sol in step 1) in the embodiment is changed to 50mL, and the rest of the steps are the same as in the embodiment 1.
[0039] The prepared mesoporous MSQ airgel / glass fiber composite material containing infrared opacifying agent has abundant pores and uniform morphology, and its thermal conductivity is 0.028 W / (m K) at room temperature and 0.092 W at high temperature (600°C). / (m•K).
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