Preparation method of adhesive for compounding mirror surface substrate
An adhesive and substrate technology, applied in the direction of adhesive types, polyurea/polyurethane adhesives, polymer adhesive additives, etc. The surface cannot be smoothed, which affects the laser effect of the card, and achieves the effect of good initial adhesion at room temperature, easy to flatten, and smooth surface.
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[0048] A preparation method of an adhesive for mirror substrate composite, comprising the steps of:
[0049] (1) Prepare the polyurethane prepolymer of modified end-NCO
[0050]Dry polytetramethylene ether glycol in vacuum at 80-90°C for 1-2 hours, cool down to 50-60°C, add dicyclohexylmethane diisocyanate to form a raw material mixture, in which dicyclohexylmethane diisocyanate and poly The mass ratio of tetramethylene ether glycol is 1:(1.5~2.0), and then the temperature is gradually raised to 80~85°C, after 1.5~2 hours of reaction, the temperature is lowered to 40~50°C, and organic bismuth catalyst, hydrophilic expansion chain agent, cross-linking agent and epoxy resin, gradually heat up to 60-65°C, then add acetone accounting for 20%-30% of the mass of the raw material mixture, react for 3-4 hours, cool down to 40-50°C, add methyl ethyl ketone oxime, Keeping the reaction at this temperature for 0.5-1 hour, raising the temperature to 65-70°C and continuing the reaction for...
Embodiment 1
[0066] Add 120 g of polytetramethylene ether glycol into a 500 ml four-neck flask, place it in a vacuum drying oven at 90° C. for 1 hour, and then cool it down to 50° C. and remove it from the drying oven. Under the protection of dry nitrogen, 80g of dicyclohexylmethane diisocyanate was added to the above-mentioned four-necked flask to form a raw material mixture, and then the temperature was gradually raised to 80°C. After 1.5 hours of reaction, the temperature was lowered to 40°C, and 0.4g of bismuth-zinc composite catalyst was added. , Hydrophilic chain extender dimethylol butyric acid 8.0g, crosslinking agent 1,4-butanediol 4.0g, trimethylolpropane 1.6g, epoxy resin 6.0g, gradually increase the temperature to 60°C, and then add 50.0g of acetone, continued to react for 3 hours. Cool down to 40°C, add 12.0g of methyl ethyl ketone oxime, keep the reaction at this temperature for 0.5 hours, raise the temperature to 65°C and continue the reaction for 1.5 hours, then cool down t...
Embodiment 2
[0075] Add 160 g of polytetramethylene ether glycol into a 500 ml four-necked flask, place it in a vacuum drying oven at 80° C. for 2 hours, and then cool it down to 60° C. and remove it from the drying oven. Under the protection of dry nitrogen, 80g of dicyclohexylmethane diisocyanate was added to the above-mentioned four-necked flask to form a raw material mixture, and then the temperature was gradually raised to 85°C. After 2.0 hours of reaction, the temperature was lowered to 50°C, and 0.96g of bismuth-zinc composite catalyst was added. , Hydrophilic chain extender dimethylol butyric acid 12.0g, crosslinking agent 1,4-butanediol 9.6g, trimethylolpropane 2.4g, epoxy resin 12.0g, gradually increase the temperature to 65°C, and then add 72.0g of acetone, continued to react for 4 hours. Cool down to 50°C, add 19.2g of methyl ethyl ketoxime, keep the reaction at this temperature for 1.0 hours, raise the temperature to 70°C and continue the reaction for 2.5 hours, then cool down...
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