Method for preparing metal and ceramic composite workpiece
A ceramic composite and metal technology, applied in the direction of metal processing equipment, manufacturing tools, ceramic molding machines, etc., can solve the problems of easy stress, high production cost, and difficulty in meeting long-term use requirements, so as to improve the bonding strength and promote combined effect
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Embodiment 1
[0023] The present invention comprises the steps:
[0024] S1, processing alumina ceramics into inserts;
[0025] S2. Ultrasonic cleaning is performed on the insert, and then preheated to 120°C;
[0026] S3, TC4 powder is mixed with binder according to the ratio of 9:1 to prepare TC4 feed; the binder is a PEG-based binder;
[0027] S4. Put the insert into the mold cavity for positioning; inject the TC4 feed into the mold cavity, and obtain a green body by injection molding;
[0028] S5, soaking the green body in pure water for 12 hours at a temperature of 50°C to obtain a degreased body;
[0029] S6, sintering the degreased body under high vacuum conditions, the sintering temperature is 1300°C, and the sintering time is 3h, and finally a metal and ceramic composite workpiece is obtained.
[0030] The bonding strength of the metal and ceramic composite workpiece prepared by the method of this embodiment is 130 MPa.
Embodiment 2
[0032] The present invention comprises the steps:
[0033] S1, processing Kovar alloy into inserts;
[0034] S2. Plasma cleaning the insert, and then preheating to 130°C;
[0035] S3, mixing glass-phase-modified zirconia ceramic powder with a paraffin-based binder in a ratio of 8.5:1 to form a ceramic feed;
[0036] S4. Put the insert into the cavity of the mold for positioning; inject the ceramic feed into the cavity of the mold, and obtain a green body by injection molding;
[0037] S5, soaking the green body in n-heptane for 13 hours at a temperature of 60°C to obtain a degreased body;
[0038] S6, sintering the degreased body under a hydrogen atmosphere, the sintering temperature is 1350° C., and the sintering time is 5 hours, and finally a metal and ceramic composite workpiece is obtained.
[0039] The bonding strength of the metal and ceramic composite workpiece prepared by the method of this embodiment is 150 MPa.
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