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Ultrahigh-toughness epoxy resin material for hot-mixed epoxy asphalt and preparation method thereof

A technology of hot-mixed epoxy asphalt and tough epoxy resin, which is applied in building insulation materials, building components, buildings, etc., to achieve the effect of increasing chain segment length and excellent phase stability

Active Publication Date: 2020-01-21
JIANGSU SINOROAD TRANSPORTATION SCI & TECH CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The main purpose of the present invention is to overcome the performance defects of the existing warm-mix epoxy asphalt, and provide a kind of ultra-high toughness epoxy resin material for hot-mix epoxy asphalt and its preparation method, prolong the construction time of epoxy asphalt , solve the compatibility problem between epoxy phase and asphalt phase in epoxy asphalt, greatly improve the bending and tension fatigue performance of epoxy asphalt, so that it is more suitable for practical use, and has industrial utilization value

Method used

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  • Ultrahigh-toughness epoxy resin material for hot-mixed epoxy asphalt and preparation method thereof
  • Ultrahigh-toughness epoxy resin material for hot-mixed epoxy asphalt and preparation method thereof
  • Ultrahigh-toughness epoxy resin material for hot-mixed epoxy asphalt and preparation method thereof

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Effect test

Embodiment 1

[0045] Embodiment 1: super high toughness epoxy resin material and preparation method thereof for hot mix epoxy asphalt

[0046] The raw materials used in this embodiment are as follows:

[0047] Polyethylene glycol monomethyl ether: MPEG-1000, Jiangsu Haian Petrochemical Plant;

[0048] Toluene diisocyanate: TDI-100, Hebei Cangzhou Dahua Group Co., Ltd.;

[0049] Bisphenol A type epoxy resin (I); DER331, U.S. Dow Chemical Company;

[0050] Toluene: industrial grade, Suzhou Kai Nuobin Petrochemical Co., Ltd.;

[0051] Bisphenol A type epoxy resin (II): DER331, American Dow Chemical Company;

[0052] Phenyl glycidyl ether: XY690, Anhui Xinyuan Technology Co., Ltd.;

[0053] 3-Glycidyl etheroxypropyl trimethylsilane: SilguestA-187, American Momentive Advanced Materials Company;

[0054] 9,11,13-octadecatrienoic acid: T160, Anhui Ruifende Oil Deep Processing Co., Ltd.;

[0055] Liquid ammonia: industrial grade, Nantong Runfeng Petrochemical Co., Ltd.;

[0056] Ammonia: 25%...

Embodiment 2

[0072] Embodiment 2: super high toughness epoxy resin material and preparation method thereof for hot mix epoxy asphalt

[0073] The raw materials used in this embodiment are as follows:

[0074] Polyethylene glycol monomethyl ether: MPEG-750, Jiangsu Haian Petrochemical Plant;

[0075] Toluene diisocyanate: TDI-80, Hebei Cangzhou Dahua Group Co., Ltd.;

[0076] Bisphenol A type epoxy resin (I): DER331, U.S. Dow Chemical Company;

[0077] Toluene: industrial grade, Suzhou Kai Nuobin Petrochemical Co., Ltd.;

[0078] Dibutyltin dilaurate: DY-12, Shanghai Deyin Chemical Co., Ltd.;

[0079] Bisphenol A epoxy resin (II): NPEL-128, Nanya Electronic Materials (Kunshan) Co., Ltd.;

[0080] Butanediol diglycidyl ether: XY622, Anhui Xinyuan Technology Co., Ltd.;

[0081] 3-Glycidyl etheroxypropyltriethoxysilane: KBE403, Japan Shin-Etsu Chemical Co., Ltd.;

[0082] Cis-12-hydroxyoctadecene-9-acid: RA-10, Anhui Ruifende Oil Deep Processing Co., Ltd.;

[0083] Liquid ammonia: indus...

Embodiment 3

[0098] Embodiment 3. super high toughness epoxy resin material and preparation method thereof for hot mix epoxy asphalt

[0099] The raw materials used in this embodiment are as follows:

[0100] Polyethylene glycol monomethyl ether: MPEG-2000, Jiangsu Haian Petrochemical Plant;

[0101] Toluene diisocyanate: TDI-60, Hebei Cangzhou Dahua Group Co., Ltd.;

[0102] Bisphenol A type epoxy resin (I): DER317, U.S. Dow Chemical Company;

[0103] Dibutyltin dilaurate: DY-12, Shanghai Deyin Chemical Co., Ltd.;

[0104] Bisphenol A epoxy resin (II): WSR6101, Bluestar Chemical New Materials Co., Ltd.;

[0105] Polyethylene glycol diglycidyl ether: XY205, Anhui Xinyuan Technology Co., Ltd.;

[0106] 3-Glycidyl etheroxypropylmethyldiethoxysilane: SCA-87F, Nanjing Nengde New Material Technology Co., Ltd.;

[0107] Cis, cis-9,12-octadecadenoic acid: L80-3, Anhui Ruifende Oil Deep Processing Co., Ltd.;

[0108] Liquid ammonia: industrial grade, Nantong Runfeng Petrochemical Co., Ltd.; ...

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Abstract

The invention discloses an ultrahigh-toughness epoxy resin material for hot-mixed epoxy asphalt and a preparation method of the ultrahigh-toughness epoxy resin material. The key points of the technical scheme are as follows: the ultrahigh-toughness epoxy resin material for the hot-mixed epoxy asphalt consists of a main agent A and a curing agent B, wherein the main agent A comprises bisphenol A epoxy resin, modified epoxy resin containing a flexible side chain, a reactive diluent and an epoxy terminated interface agent; the curing agent B comprises following components in parts by weight: long-chain fatty primary amine and an accelerant. The crosslinking density of an epoxy cured product is controlled by synthesizing monofunctional long-chain fatty primary amine, and finally, the operabletime of the hot-mixed epoxy asphalt material is longer than 2 hours; the compatibility problem between an asphalt phase and an epoxy phase is solved on the basis of a 'reaction induced phase splitting' technical principle; by introducing the modified epoxy resin containing the flexible side chain, the fatigue resistance of the hot-mixed epoxy asphalt material is greatly improved.

Description

technical field [0001] The invention relates to a hot-mix epoxy asphalt material, in particular to an ultra-high toughness epoxy resin material for hot-mix epoxy asphalt and a preparation method thereof. Background technique [0002] In the past 20 years, my country's long-span steel box girder bridges have entered a period of rapid construction. However, the development speed of long-span steel bridge deck pavements is far from meeting the actual needs of high temperature, rainy, and heavy loads in China. Paving materials such as epoxy asphalt have been found to have various degrees of disease after 3 to 5 years of use. In view of the strict high and low temperature performance requirements and strict bending and tensile fatigue performance requirements of steel bridge deck pavement, epoxy asphalt has always been the first choice for long-span steel bridge deck paving at home and abroad because of its unique microstructure and wide performance plasticity. material of choice...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L63/00C08L95/00C08G59/50
CPCC08G59/5013C08L63/00C08L95/00C08L2205/025
Inventor 陈李峰潘友强李款张志祥
Owner JIANGSU SINOROAD TRANSPORTATION SCI & TECH CO LTD
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