Magnolia bark gel beads for smoking
A technology of gel beads and Magnolia, applied in the application, tobacco, smoke oil filter and other directions, can solve the problems of high porosity, easy loss of essence, poor adsorption and diffusion efficiency, etc. The effect of improving the encapsulation rate
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Embodiment 1
[0025] Preparation of magnolia volatile oil: crush 100g of magnolia bark into pieces of about 2mm-10mm; add 300-500g of distilled water, soak at room temperature for 8-24h, heat and reflux at 85°C under normal pressure for 1-5h, and collect the distillate with a condenser The liquid is discharged, and the oil and water are separated to obtain Magnolia officinalis volatile oil.
Embodiment 2
[0027] Get 0.5g Magnolia officinalis volatile oil and dissolve in 10g propylene glycol, the propylene glycol solution of Magnolia officinalis volatile oil is 0.3g / ml low methoxy pectin solution, 100ml concentration is the guar gum solution of 0.5g / ml to mix with 100ml concentration, add 0.5g Span-80, homogenize at 85-95°C for 5min, adjust pH to 7, stir evenly, add 10g additive sodium stearate, vacuumize to remove air bubbles, cool to 4°C, add dropwise at a rate of 2ml / min 100ml of calcium chloride solution with a concentration of 0.2g / ml was added dropwise while stirring, 60g of polyethylene glycol was added, and the cross-linking reaction was carried out for 1 hour to obtain pre-composite gel beads;
[0028] Add 20ml of sodium tetraborate solution with a concentration of 0.1g / ml, solidify at room temperature for 1 hour, and filter. The aperture of the sieve is 1-5mm to obtain composite gel beads;
[0029] Blot dry the moisture on the surface of the composite gel beads and tra...
Embodiment 3
[0032] Get 5g magnolia volatile oil and dissolve it in 20g propylene glycol, the propylene glycol solution of magnolia volatile oil and 100ml concentration are 0.5g / ml low methoxyl pectin solution, 100ml concentration is 1g / ml guar gum solution, add 0.5g Class-80, homogenize at 85-95°C for 5 minutes, adjust the pH to 7, stir evenly, mix evenly at 85-95°C, stir evenly, and add 20g of additive sodium stearate, vacuumize to remove air bubbles and cool to 4°C to Add 100ml of calcium chloride solution with a concentration of 0.4g / ml dropwise at a speed of 2ml / min, stir while adding dropwise, add 80g of polyethylene glycol, and cross-link for 1 hour to obtain pre-composite gel beads;
[0033] Add 20ml of sodium tetraborate solution with a concentration of 0.1g / ml, solidify at room temperature for 1 hour, and filter. The aperture of the sieve is 1-5mm to obtain composite gel beads;
[0034] Blot dry the moisture on the surface of the composite gel beads and transfer to 100 ml of chit...
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